NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\FEB1302\30648.D Vial: 14
Acq On : 14 Feb 2002 3:48 am Operator: 209 GALOS
Sample : GC/MS SCAN Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 11 Benzoic acid, 2,5-bis(trimethy Concentration Rank 12
R.T. EstConc Area Relative to ISTD R.T.
29.35 0.49 ug/1 233389 Phenanthrene-dl0 25.77
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Benzoic agid, 2,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 35
2 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 35
3 3-Isopropoxy-1, 1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 25
4 N-(Tri uoracetyl)-0,0',0"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 17
Abundance > Scan 2648 (29.350 min): 30648.D (-) m/ Z 73.Q0 100.00%
73
5000 147
221 281 355 1 ' I ' 1 1 । 1 > > > । ■
29.00 29.20 29.40 29.60
45 .
■ ■ ‘ i ’> ■
117. ,1 191 |, 249 ,
1 "I1 r 1 ■‘
327 I I 401 429
> T > ■> v ■ I > ■ ■ • I ■ 1 । > I ■ > m/z 147.00 37.10%
m/z~> 50 100 150 200 250 300 350 400 450 500 550
Abundance #73978: Benzoic acid, 2,5-bis(trimethylsiioxyj-, trimethyls
73
355
5000 ■ ■ i 1 ■ 1 1 1 1 ' 1 1 1
29.00 29.20 29.40 29.60
45 m/ z 355.05 20.66%
...... ........ 147 179 223 267,297.......,..............................
m/z-__ 50
Abundance
100
1- A
150 200 250 300 350 400 450 500 550
73 147 ......... /
—.ru । । । । । ।
—i l 1 ' 11 1 1 1 » 1
281 29.00 29.20 29.40 29.60
5000- m/z 221.05 20.21%
207 249 369
........... :......... 249 ..... 338
m/z-> . 50... 100___ 150__ 200__ 250 300 350 400 .450 500 550
Abundance #60503: 3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3.5.5-tris(trim 1 ' i ■ 1 ■ ■ । 1 < r1 1 1 1 1 1 1 1
73 29.00 29.20 29.40 29.60
m/z 281.0.0 18.85%
5000
147
221 281 39- E
........................... [.......... !. 415 519 561 ...... .................
50 100 150 200 250 300 350 400 450 500 550 29.00 29.20 29.40 29.60
30648.D GCMS0103.M Thu Feb 14 11:02:06 2002 Page 11
NYC-WTC_000004488
OCR can misread numbers and units. Confirm readings against the page image before using them.