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Document / 344 pages

DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004149–000004492

Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB1302\30648.D Vial: 14 Acq On : 14 Feb 2002 3:48 am Operator: 209 GALOS Sample : GC/MS SCAN Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 Benzoic acid, 2,5-bis(trimethy Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

29.35 0.49 ug/1 233389 Phenanthrene-dl0 25.77

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzoic agid, 2,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 35 2 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 35 3 3-Isopropoxy-1, 1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 25 4 N-(Tri uoracetyl)-0,0',0"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 17 Abundance > Scan 2648 (29.350 min): 30648.D (-) m/ Z 73.Q0 100.00% 73

5000 147 221 281 355 1 ' I ' 1 1 । 1 > > > । ■ 29.00 29.20 29.40 29.60 45 . ■ ■ ‘ i ’> ■ 117. ,1 191 |, 249 , 1 "I1 r 1 ■‘ 327 I I 401 429 > T > ■> v ■ I > ■ ■ • I ■ 1 । > I ■ > m/z 147.00 37.10% m/z~> 50 100 150 200 250 300 350 400 450 500 550 Abundance #73978: Benzoic acid, 2,5-bis(trimethylsiioxyj-, trimethyls 73 355

5000 ■ ■ i 1 ■ 1 1 1 1 ' 1 1 1 29.00 29.20 29.40 29.60 45 m/ z 355.05 20.66% ...... ........ 147 179 223 267,297.......,.............................. m/z-__ 50 Abundance 100 1- A 150 200 250 300 350 400 450 500 550 73 147 ......... / —.ru । । । । । । —i l 1 ' 11 1 1 1 » 1 281 29.00 29.20 29.40 29.60 5000- m/z 221.05 20.21%

207 249 369 ........... :......... 249 ..... 338 m/z-> . 50... 100___ 150__ 200__ 250 300 350 400 .450 500 550 Abundance #60503: 3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3.5.5-tris(trim 1 ' i ■ 1 ■ ■ । 1 < r1 1 1 1 1 1 1 1 73 29.00 29.20 29.40 29.60 m/z 281.0.0 18.85% 5000 147 221 281 39- E ........................... [.......... !. 415 519 561 ...... ................. 50 100 150 200 250 300 350 400 450 500 550 29.00 29.20 29.40 29.60

30648.D GCMS0103.M Thu Feb 14 11:02:06 2002 Page 11

NYC-WTC_000004488

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NYC-WTC_000004488Source: NYC Law Department, mirrored locally

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