DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB1302\30648.D Vial: 14 Acq On : 14 Feb 2002 3:48 am Operator: 209 GALOS Sample : GC/MS SCAN Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 10 Dibutyl phthalate Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

27.72 0.36 ug/1 171276 Phenanthrene-dl0 25.77

Hit# of 5 Tentative ID MW MolForm CAS# Qual

Dibutvl phthalate 2 Bis (2 -methoxyethyl ) phthalate 278 C16H2204 282 C14H1806 000084-74-2 000117-82-8 91 83 3 1,2-Benzenedicarboxylic acid, bis(2 278 C16H2204 000084-69-5 78 4 J. , 2-Benzenedicarboxylic acid, dipro 250 C14H1804 000131-16-8 72 Abundance Scan 2470 (27,716 min): 30648.D (-) m/z 149.00 100.00% 149

5000 1....... , 27.40 27.60 27.80 28.00 41 53. 65 76 93 104 121132 160 205 223 1 * i’■ 1* । । . । t । . . i’ । । r । । । f i j T > [ . । . > . . । । । । | . > r ■ i ■ ■ 1 ■ । ■ 1 11 1 m/ z 150.00 8.74% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #72214: Dibutyl phthalate 149

5000 ■ ■ । ■ ' 1 i ■ ■ ' ■ i 27.40 27.60 27.80 28.00 m/z 41.05 8.25% 41 56 76 93 104 121 205 223 278 ‘ I‘ 111 m/Z-2_____ 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance 149 TITRPTTTTTITTI 27.40 27.60 27.80 28.00 5000 m/ z 76.00 6.39%

41 57 76 93 1 04 121 ' 160 205 223 1 1 I ' m/z-> 40 60__ 80 100 120__140 160 180 200 220 240 260 280 .... ......... Abundance #72217:1,2-Benzenedicarboxyiic acid, bis(2-methylpropyij e ‘ I’’ 149 27.40 27.60 27.80 28.00 m/z 103.95 5.36% 5000 57 163 r , I1, . . 76 . 93 104 121132 45 1 1 1 1 194205 236 . 278 280 1 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 27.40 27.60 27.80 28.00

30648.D GCMS0103.M Thu Feb 14 11:02:02 2002 Page 10

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