GCMS analysis results for sample AD31406, Feb 2002

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Laboratory report documenting GCMS analysis of sample AD31406 conducted on February 13, 2002.

NYC-WTC_000018362–000018372

Folder label: “GCMS X 12/27/01 A 1/16/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\JAN1602\31406.D Vial: 13 Acq On : 16 Jan 2002 11:22 pm Operator: 209 GALOS Sample : gc/ms scan 12/27 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1,2-Benzenedicarboxylic acid, Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T.

26.80 0.22 ug/1 65248 Phenanthrene-dl0 24.77

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,2-Benzenedicarboxylic acid, dipro 250 C14H18O4 000131-16-8 78 2 1,2-Benzenedicarboxylic acid, butyl 278 C16H2204 017851-53-5 78 3 1,2-Benzenedicarboxylic acid, bis (2 278 C16H22O4 000084-69-5 78 (4) Dibutyl phthalate 278 C16H2204 000084-74-2 78 Abundance ~ Scan 2370 (26.798 min): 31406.D (-) m/z 149.00 1 00.00% 149

5000

26.40 26.60 26.80 27.00 27.20 *41 57. 76 .124 1?2 I 205 223 m/z 41.05 9.67% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #71449:1,2-Benzenedicarboxylicacid, dipropyl ester 149

5000 PM MM1 444 26.40 26.60 26.80 27.00 27.20 m/z 150.00 8.75% 43 56 76 104 121 | 191 209 1 , , 4 । ' , |. ,—+— T A,—I—t—!—I—J—1—{—|—I—I—I—1—1——— 250 m/z-s 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39'31' 1.2-Benzanularboyyit 0d. cuti 2-0 59y Iprop. 149

26.40 26.60 26.80 27.00 27.20 5000 m/z 103.95 7.49%

27 41 57 76 104 121 205 223 278 11 1 ' 1 1 1 ‘ ■ i 1 ■ ‘ ■ I ■ ‘ ■ i ' ■ ■ ■ i ■ ■ ‘ • i1 ‘ 1 ■ i ■ • ' ■ i ■ ■ ' ■ i • ■ ■ ' i ■ ■ ■ ‘ i ■ ' • ■ i' • ■ ■ i ■ m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39134:1.2-Benzenedicarboxylic acid. bis(2-methylpropy!) e T • I • » 149 26.40 26.60 26.80 27.00 27.20 m/z 76.00 5.74% 5000

57 223 1 .. 76 ’...... . . 167. ........205. ' 104 121 i ■ ■ ■ ■ i ■ ■111 ■‘ • • 1 i ' ‘ | i » t . । । . . । । । r. . । t » I 236 । । * । ijn ■ ■ i1 ■ ■ ■ i ■ ■ ■ 278 miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 26.40 26.60 26.80 27.00 27.20

31406.D GCMS0103.M Thu Feb 07 09:15:52 2002 Page 3

NYC-WTC_000018371

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