GCMS analysis results for sample AE01937 with surrogate data, Feb

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\FEB0802\1937.D Vial: 17 Acq On 9 Feb 2002 12:53 am Operator: 209 GALOS Sample GC/MS SCAN 1/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1,2-Benzenedicarboxylic acid, Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

27.71 0.24 ug/1 23746 Phenanthrene-dl0 25.76

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,2-Benzenedicarboxylic acid, butyl 278 C16H2204 017851-53-5 83 hthalate ) 278 C16H2204 000084-74-2 83 3 1,2-Benzenedicarboxylic acid, dipro 250 C14H1804 000131-16-8 78 4 1,2-Benzenedicarboxylic acid, butyl 334 C20H30O4 000085-69-8 64 Abundance Scan 2469 (27.713 min): 1937.D (-) m/ z 149.0,0 100.00% 1 -9

5000

41 56 76 104 121 205 223 27.40 27.60 27.80 28.00 IE IIPIPPP m/z 149.90 9.51% m/Z-2.... 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39131: 1,2-Benzenedicarboxylic acid, butyl 2-methylpropyl 149

I 1 5000 27.40 27.60 27.80 28.00 m/z 41 • 0.5 8.18% 27 41 57 76 104 121 1 | । > ■ । f ' 1 ■ 1 !■ | > 1 U । | 1 । 1 > | I 1 1 205 2?3 278 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance 149

27.40 27.60 27.80 28.00 5000 m/z 103.95 6.97%

41 56 76 104 -121 205 223 278 m/z~> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #33901: 1,2-Benzenedicarboxylic acid, dipropyl ester 149 27.40 27.60 27.80 28.00 m/z 75.90 6.70% 5000

31 43 56 76 11 i ■ ■ । |''i >•■ । । i' ■ । 1 ] 1 । 104 1 r - 1121 167 191 209 [ ‘ ‘I* ■ ■ > । i । । । । > > । ■ । • > < i [ । ■ ■ ' । > > । ■ । > । > > । । m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 27-40 27.60 27.80 28.00

1937.D GCMS0208.M Thu Feb 14 15:00:39 2002 Page 1

NYC-WTC_000003846