GCMS analysis results for sample AE02597, Mar 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\MAR0102\2597.D Vial: 7 Acq On 1 Mar 2002 2:15 pm Operator: Sample gc/ms scan 2/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 1,2-Benzenedicarboxylic acid, Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

27.69 0.24 ug/1 28249 Phenanthrene-dl0 25.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,2-Benzenedicarboxylic acid, butyl 304 C18H24O4 000084-64-0 83 2 Dibutyl phthalate 278 C16H2204 000084-74-2 (83 3 1,2-Benzenedicarboxylic acid, butyl 278 C16H2204 017851-53-5 83 4 1,2-Benzenedicarboxylic acid, dipro 250 C14H1804 000131-16-8 78 Abundance Scan 2467 (27.687 min): 2597.D (-) 1 -9 m/z 149.00 100.00%

5000 -r-r-f-r-r ' ' I 1 ' 41 57 76 104 121 27.40 27.60 27.80 28.00 .1 205 223 I ' ' ' ' I ' ' । r। । - । I । i i r■ । I । । m/z 149.90 9.52% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #43452: 1,2-Benzenedicarboxylicacid. butyl cyclohexyl ester 149

5000 27.40 27.60 27.80 28.00 m/ z 40.95 8.70% ■........ 55 67 83 104 . ........ . 167 205 223 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance .. 149

27.40 27.60 27.80 28.00 5000 m/z 103.95 5.62%

41 56 76 104 121 205 223 278 m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39131: 1,2-Benzenedicarboxylicacid, butyl 2-rnethylpropyI 1 19 27.40 27.60 27.80 28.00 m/z 223.00 5.08% 5000

■ 27 41 57 76 104 121 205 2?3 278 । । TTI ■ rr ----- ■ r1 ‘ ‘I‘ 1 ■ ■ । • ■ ’ ■ । ‘ ।1111 r1'1111 ■11111111' m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 27.40 27.60 27.80 28.00

2597.D GCMS0208.M Mon Mar 04 11:41:28 2002 Page 3

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