GCMS analysis results for sample AD31592, Feb 28 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB2102\31592.D Vial: 42 Acq On : 23 Feb 2002 7:32 am Operator: Sample : gc/ms scan 2/21 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library . : C:\DATABASE\NBS75K.L

Peak Number 2 1,2-Benzenedicarboxylic acid, Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

34.01 0.28 ug/1 18545 Chrysene-dl2 33.80

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

nzenedicarboxylic acid, diiso 390 C24H3804 027554-26-3.83 ,2-Benzenedicarboxylic acid, 3-nit 211 C8H5NO6 000603-11-2 72 3 is(2-ethylhexyl) phthalate 390 C24H3804 000117-81-7 72 4 1,2-Benzenedicarboxylic acid, mono( 278 C16H22O4 004376-20-9 64 'Abundance Scan 3155 (34.010 min): 31592.D (-) m/z 149.00 100.00% 149

5000 57 167 43 70 —— -1 83 113 236 279 33.60 33.80 34.00 34.20 34.40 | 207 - ............ I m/z 57.0,0 35.48% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #53134: 1,2-Benzenedicarboxylic acid, diisooctyl ester 149

5000 57 70 167 33.60 33.80 34.00 34.20 34.40 I m/z 167.00 32.30% I 279 ' ' i ' ' ' ' 183 ' i ' ' ' ' i ' • ' ' 104 121132 i ' ' ' ' i ' ■ 1 ■ i ' ' —......... - — m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #25513: 1,2-Benzenedicarboxyiic acid. 3-nitro- 149 i ■ ■ ' ■ i • ' ■ ■ i 33.60 33.80 34.00 34.20 34.40 5000- m/z 43.0,5 25.40% 167 71 : 83 113 132 1 , .......................... ———————— m/z-> 40 60 80 100 120 140 160__ 180 200 220 240 260 280 'Abundance #53128: Bis(2-ethylhexyl) phthalate 149 33.60 33.80 34.00 34.20 34.4C m/ z 4 0.95 24.35% 5000 57 167 71 I 83 113 279

m/z-> — 1 H— —132— , ■ ■ i ■ 40 I............................- ----I 60 80 100 120 140 160 180 200 220 240 260 280 33.60 33.80 34.00 34.20 34.40

31592.D GCMS0208.M Wed Feb 27 12:07:28 2002 Page 2

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