GC/MS calibration data for sample 30647, Dec 2001

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Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.

NYC-WTC_000018546–000018575

Folder label: “GCMS X 12/18/01 A 12/30/01”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30706.D Vial: 54 Acq On : 30 Dec 2001 12:10 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 Bis(2-ethylhexyl) phthalate Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

33.30 0.34 ug/1 135965 Chrysene-dl2 33.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

Bis(2-ethylhexyl) phthalate 390 C24H3804 000117-81-7 87 1,2-Benzenedicarboxylic acid, 3-nit 211 C8H5NO6 000603-11-2 87 3 1,2-Benzenedicarboxylic acid, diiso 390 C24H3804 027554-26-3 53 4 Di-n-octyl phthalate 390 C24H3804 000117-84-0 52 Abundance Scan 3078 (33.299 mln): 30706.D (-) m/z 148.95 100.00% 149

5000 43 57 167 71 t j i । » t pv t । t 11′4 1 I ri IPs

miz-> —11,95,113,122— 40 60 80 100 120 TIr • i ■ ■ ■ ■ i 207 228 279 • '■ ■ • i ‘1 ■ ri1 ■1 ' i ■ - 140 160 180 200 220 240 260 280 m/z 33.00 33.20 33.40 33.60 57.00 34.17% Abundance #53128: Bis(2-ethylhexy) phthalate 149

5000 III"TT T T 57 167 33.00 33.20 33.40 33.60 71 m/z 167.00 29.23% I 83 113 __ 279 • ■ । ■ i p A11 'i । | • r> 132 । । i p ri । । 1"" • i ■ ■ • ■ i • • • ■ i ■ ■ ■11111 • i ‘ • i ■ ■ miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #25513: 1.2-Benzeredicarboxylicacid. 3-nitro- 149 • • i • 1 1 i 1 1 33.00 33.20 33.40 33.60 5000 m/z 43.00 27.01% 167 71 : 83 113 132 | d 1 -r-p-r-n-p-T m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #53134:1,2-Benzenedicarboxylic acid, diisooctyl ester 149 33'o6 33.20 33.40 33.60 ___ m/z 41.05 24.10% 5000 57 167 70 83 104 , 279

m/z-> ---132 ■ ■ i ■ • ■11 ■ 40 60 1......... . ........................ I,,, i • • ■ ‛14‛•41****111**I*1*‛I+‛‛+I**‛*I** 80 100 120 140 160 180 200 220 240 260 280 T 1AUIW4411II

33.00 33.20 33.40 33.60

30706.D GCMS1126.M Fri Feb 01 11:08:48 2002 Page 13

NYC-WTC_000018573

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