Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
NYC-WTC_000018546–000018575Folder label: “GCMS X 12/18/01 A 12/30/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC2701\30706.D Vial: 54 Acq On : 30 Dec 2001 12:10 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 3-Isopropoxy-l,1,1,7,7,7-hexam Concentration Rank 11
R.T. EstConc Area Relative to ISTD R.T. 31.72 0.54 ug/1 218151 Chrysene-dl2 33.02 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 42 2 Ethanedioic acid, bis (trimethylsily 234 C8H18O4S12 018294-04-7 38 3 Trisiloxa:ne, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 23 4 1,1,1,5,7 ,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 23 Abundance Scan 2906 (31.720 min): 30706.D (-) " 73.oo 100.00% 73
5000 147 221 204i1 355 490 l । । r t <1 > Tgin n i i I3i j
191 [ 249 I . 325, L 401 i 31.40 31.60 31.80 32.00 45 117 ■ -IT m/z 146.95 42.96% mz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-!sopropoxy-1,1,1,7,7,74iexamethyl-3,5,5-trls(trim 73
5000 T T T T ‘I 147 31.40 31.60 31.80 32.00 221 281 3= 4= m/z. 221.0.5 22.50% 1 -11—99990—* I 327, 415 519 561 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #71006: Ethanedioic acid, bis(trimethylsily!) ester 73 147 .. A... I • I I 1 1 1 J II > 31.40 31.60 31.80 32.00 ydd 1 1 1 l 1»» }
5000 m/z 281.00 16.14% 45 ....... 117 1 190 219 miz-> 50 100 150 200 250 300 350 400 450 500 550" Abundance #74103: Trisiloxane, 1,1,1,5.5,5-hexamethyl-3,3-bis[(trimet 73 31.40 31.60 31.80 32.00 147 m/z 355.05 12.09% 5000 281 45
m/z-> 4 50 117 41*** 100 150 ,4....2%7 249, . ............. ..। 200 250 300 350 369
400 450 500 550 T —A 31.40 31.60 31.80 32.00 T T
30706.D GCMS1126.M Fri Feb 01 11:08:43 2002 Page 12
NYC-WTC_000018572
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NYC-WTC_000017675
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30251 conducted on January 9, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017833
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017724
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30426 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017782
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD303B5 conducted on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017808
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30352 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000004149
Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036712
GCMS analysis report for sample AD29563 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036798
GCMS analysis report for sample AD29523 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034988
Laboratory report noting contamination from the TurboVap concentrator and recovery rates for sample AD28662.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000018416
Single-page document containing GCMS data or metadata associated with the WTC site in December 2001.
Filed in the same folder
NYC-WTC_000018417
Laboratory log sheet detailing Method 508 extraction and analysis parameters for samples processed in December 2001.
Filed in the same folder
NYC-WTC_000018420
Laboratory report documenting GCMS blank analysis of sample AD30643 conducted on February 1, 2002.
Filed in the same folder
NYC-WTC_000018436
Laboratory report documenting GCMS calibration data for sample AD30643 conducted on February 1, 2002.
Filed in the same folder
NYC-WTC_000018440
Laboratory report documenting GCMS reference analysis of sample AD30643 conducted on February 1, 2002.
Filed in the same folder