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← Document results/DEP Box 16/GCMS X 12/18/01 A 12/30/01
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GC/MS calibration data for sample 30647, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.

NYC-WTC_000018546–000018575

Folder label: “GCMS X 12/18/01 A 12/30/01”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30706.D vial: 54 Acq On : 30 Dec 2001 12:10 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 1-Monolinoleoylglycerol trimet Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T.

30.25 0.70 ug/1 282378 Chrysene-dl2 33.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1 -Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 45 2 2-Hexenedioic acid, bis(trimethylsi 288 C12H2404Si2 055494-10-5 23 3 Butanoicacid, 3 -methyl-2 -[ (trimeth 262 CllH26O3Si2 055124-92-0 23 4 Ethanedioic acid, bis (trimethylsily 234 C8H18O4Si2 018294-04-7 23 Abundance Scan 2746 (30.251 mln): 30706.D (-) m/ z 73.00 100.00% 73

5000 147 221 281 355 .nn M 30.00 30.20 30.40 30.60 45 L, ’ 327 95 117 „ 4., mij 1, 251-1*} [ 401 i TIT i “4 PI“’tt "F"I r t j j j m/z 147.00 38.25% mlz-> 50 100 150 ' ' 200 ‘ ' 250 ‘ 300 350 400 450 Abundance #58871: 1-Monolinoleoyiglycerol trimethylsilyl ether 73

5000 147 207 =. Nr... . .. 30.00 30.20 30.40 30.60 34 103 m/z 221.05 21.05% ii i 281 I 395 ■ 1 i • ■ ■ • I 1 ........ . .............................. ............... ‘ 1 i ‘ 482 ‘ • miz-> 50 100 150 200 250 300 350 400 450 Abundance #40777. 2-Hexenedioic acid, bis(trimethylsilyi) ester, (E)- 73 T-r-j-r T T T 30.00 30.20 30.40 30.60 5000 m/z 355.05 14.48% 147 45 |.I, 112 ‘244 273 miz-> 50 100 150 200 250 300 350 400 450 Abundance #71782: Butanoic acid, 3-methyl-2-[(trimethylsilyi)oxy}-, t • * 1 * ■ I 1 1 73 30.00 30.20 30.40 30.60 145 m/z 281.00 13.25% 5000

45 I. । I 117 , , 190 219 247 • * i • ■ ■ • I • ‘ ' • i ■ m/z—> 50 100 150 ‘ 200 ‘ 250 ' ‘300 350 ‘ ‘460' '' 450 30.00 30.20 30.40 30.60

30706.D GCMS1126.M Fri Feb 01 11:08:39 2002 Page 11

NYC-WTC_000018571

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NYC-WTC_000018571Source: NYC Law Department, mirrored locally

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