GC/MS calibration data for sample 30647, Dec 2001

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Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.

NYC-WTC_000018546–000018575

Folder label: “GCMS X 12/18/01 A 12/30/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC2701\30706.D Vial: 54 Acq On : 30 Dec 2001 12:10 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 1-Monolinoleoylglycerol trimet Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 28.65 0.57 ug/1 331102 Phenanthrene-dl0 24.98 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 42 2 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 32 3 3-Isopropoxy-1, 1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 25 4 Benzeneethanamine, N-[ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 16 Abundance Scan 2572 (28.654 min): 30706.D (-) m/z 73.00 100.00% t 73

5000 147 221 281 355 251 325 401 429 28.40 28.60 28.80 29.00 45 ■ ’’I' 1 117 ■ r4 ri i 1" *1"1 i rfipu [ »i।।।।i।।।■।।i। m/z 147.00 36.33% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58871:1-Monollnoleoylglycerol trimethyisilyl ether 73

207 V 5000 147 4144/4/4**1/** 28.40 28.60 28.80 29.00 34 103 I 281 m/z 221.0 19.97%

m/z—> 50 *’ 100 150 ‘1200 250 .......... .395..... 482... 300 350 400 450 500 550 Abundance #52459: Trisiloxane, 1,1.1.5,5.5-hexamethyl-3,3-bis[(trimet 73 147 / \ T T I * ‘ * U 281 28.40 28.60 28.80 29.00 5000 m/z 355.0 18.32% 369 207 249 ■ ■ i ■ ■ ■ ■ i • ■ 1 11 t ■ ■ ■ 338.......... miz-> 50 100 150 200 250 300 350 400 450 500 ‘ 550 Abundance #60503:3-Isopropoxy-1 ,1,1,7,7,7-hexamethyl-3,5,5-tris(trim ' ‘ i ‘ ‘ I' ■1 ■ i • ■ • • i ‘ ' 73 28.40 28.60 28.80 29.00 m/z 281.00 15.49% 5000 147 221 241 415 519 561 _ _______ /___________ **I**I*IIIIIII m/z~> 50 100 150 200 250 300 350 400 450 500 550 28.40 28.60 28.80 29.00

30706.D GCMS1126.M Fri Feb 01 11:08:34 2002 Page 10

NYC-WTC_000018570

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