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GC/MS calibration data for sample 30643, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.

NYC-WTC_000018445–000018469

Folder label: “GCMS X 12/18/01 A 12/30/01

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Scanned page image, NYC-WTC_000018460
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC2701\30643.D Vial: 59 Acq On : 30 Dec 2001 5:02 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 1-Monolinoleoylglycerol trimet Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

26.88 2.45 ug/1 1801080 Phenanthrene-dl0 24.98

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 42 2 Trisiloxane, 1,1,1,5,5, 5-hexamethyl 384 C12H36O4Si5 003555-47-3 35 3 3 - Isopropoxy-1,1,1,7, 7,7-hexamethyl 576 C18H5207Si7 071579-69-6 34 4 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 32 Abundance Scan 2379 (26.883 min): 30643.D (-) m/z 73.00 100.00% 73

5000 147 J \ 221 281 45 249 [ 327355 401 429 26.60 28.80 27.00 27.20 0- 117 . 191 [ । 1 i-i ri’l । it Pi” ; • ■ j T*mmer t ■ । • ■ ■ • । . • • ■ । ■ • m/z 147.00 31.94% ** i ' m/z-> 50 100 150 200 250 300 350 400 450 500 KO Abundance #58871:1-Monolinoleoylglycerol trimethylsilyl ether 73

207 5000 147 34 I 26.60 26.80 27.00 27.20 103 i 281 m/z 281.00 16.12% 41 l il ----- 482 miz-> 50 100 150 200 250 300 350 400 450 500 ’ 550 Abundance #52459; Trisiloxane, 1 1.1.5,5,5-hexamethyl-3.3-bis[(trimet 73 147 281 26.60 26.80 27.00 27.20 5000 m/z 221.05 14.92% 369 207 249 338 j m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #80503:3-lsopropoxy-1t1,1,7,7,7-hexamethyl-3,5,5-tris(trim - 73 26.60 26.80 27.00 27.20 m/z 74.00 8.22% 5000 147 221 281 327 415 519 561 ‘ > i • • > ■ l • • ■ • i • • • • l ‘ r • • l • 1 T rin f I r > i i | ili i i|i i rm i * i 1 i ‘ ■ m/z-> 50 100 150 200 250 300 350 400 450 500 550 26.60 26.80 27.00 27.20

30643.D GCMS1126.M Fri Feb 01 10:48:22 2002 Page 10

NYC-WTC_000018460

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NYC-WTC_000018460Source: NYC Law Department, mirrored locally

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