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GC/MS calibration data for sample 30643, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.

NYC-WTC_000018445–000018469

Folder label: “GCMS X 12/18/01 A 12/30/01

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Scanned page image, NYC-WTC_000018459
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30643.D Vial: 59 Acq On : 30 Dec 2001 5:02 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Benzeneethanamine, N-[(pentafl Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

22.79 4.70 ug/1 3453540 Phenanthrene-dl0 24.98

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzeneethanamine, (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 35 2 Benzoic acid, 2,6- s (trimethylsil 370 C16H30O4Si3 003782-85-2 32 3 3-1 sopropoxy-1,1, ,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 28 4 Benzoic acid, 2, -bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 25 Abundance Scan 1933 (22.789 min): 30643.D (-) m/z 73.0.0 100.00% 73

5000 147 355 221 281 22.40 22.60 22.80 23'00 23.20 r j f 1 T1"I " rtrp ,* .401, 441 ....... 45 249. I 327 | 0- — 1" 117 fad/numu191, 191,A ri * ....................... ■ • F• • ■ ■ i ■ ■ ■ 1 l 1 1 1 1 I ' 1 m/z 355.0 27.66% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methylene] 73 355

5000 22.40 22.60 22.80 23.00 23.20 45 m/z 147.00 27.45% I. 208 251.281 388 458 548 ‘ 11 1 r' » । * • ' * । * » • ' । • i •'» 11 i ■ • ■ ■ i • ■ • ■ i • ■ ‘ ‘ I • 1 1 1 I 1 1 ' 1 1 1 1 miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51296; Benzoic acid, 2.6-bis[(trimethylsilyl)oxy]-. trimet 73 355 I***I* 1 1 1 1 1 1 1 ' 1 1 1 22.40 22.60 22.80 23.00 23.20 5000 m/z 221.05 19.08% 147 267 47 208 237 t , 1 1 I ‘ ■ i ■ • • ■ i••■•i‘■■■I■■■•i‘1‘‘i■1 ■ ■ i ' ' ■ ■ i ' ■ ■ ■ i ‘ • i ■ ■ miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim ■ i ■ • ■ ■ i • ■ ■ ■ i 1 • ■ ■ i 1 1 • ■ i • ■ 73 22.40 22.60 22.80 23.00 23.20 m/z 281.00 14.90% 5000 147

1 1 1 1 ' 221 21 327 415 * I » » rra » J r | j r » »" |"i 1 r-r] sst f । > » । » । « । » r । 1 1 1 r । j 519 561 1 mrnt ’IaBaITIIIT148 m/z-> 50 100 150 200 250 300 350 400 450 500 550 22.40 22.60 22.80 23.00 23.20

30643.D GCMS1126.M Fri Feb 01 10:48:17 2002 Page 9

NYC-WTC_000018459

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NYC-WTC_000018459Source: NYC Law Department, mirrored locally

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