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Document / 344 pages

DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004149–000004492

Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02

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Scanned page image, NYC-WTC_000004421
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC27O1\3O641 .D Vial: 42 Acq On : 29 Dec 2001 11:33 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Benzeneethanamine, N-[(pentafl Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

22.79 3.41 ug/1 2187640 Phenanthrene-dl0 24.99

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Benzeneethanamine, N- [ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 35 2 Benzoic acid,/2,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 25 3 N-(Trifluoroacetyl)-N,O,O',O''-tetr 553 C22H42F3NO4Si4 000000-00-0 22 4 Benzoic a Gid, 2,6-bis[(trimethylsil 370 C16H3004Si3 003782-85-2 20 Abundance Scan 1933 (22,791 min): 30641 .D (-) m/z 73.00 100.00% ! 73 I

5000 147 355 221 281 1 45 0- ' ■'I I 1 117. 191 , 249 , | *IMIITIPITIT 327 491.443 22.40 22.60 22.80 23.00 23.20 m/z 147.00 26.97% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyljmethylene] 73 355

5000 22.40 22.60 22.80 23.00 23.20 45 m/z 355.05 26.96% , J , I.. . 208 251 281 1 386 458 ..... 548 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance 473975. Benzoic cid 2 S-bistimelllgtosy)-, trimnethyis 73 355 22.40 22.60 22.80 23.00 23.20 5000 m/z 221.05 19.37% 45 147 179 223, ............................................ m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60162: N-(Trifluoroacetyl)-N,O,O',O"-tetrakis(trimethylsi 73 22.40 22.60 22.80 23.00 23.20 m/z 281.00 15.05% 355 5000

45 147 193 267 ( I ........ 538 , , Iu ’ 1 m/z-> 50 100 150 200 250 300 350 400 450 500 550 22.40 22.60 22.80 23.00 23.20

30641.D GCMS1126.M Mon Jan 28 11:14:10 2002 Page 7

NYC-WTC_000004421

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NYC-WTC_000004421Source: NYC Law Department, mirrored locally

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