NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2 701\30641.D Vial: 42
Acq On : 29 Dec 2001 11:33 pm Operator: 209 GALOS
Sample : GC/MS SCAN 12/18 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 6 Benzoic acid, 4-ethoxy-, ethyl Concentration Rank 12
R.T. EstConc Area Relative to ISTD R.T.
21.03 1.28 ug/1 747086 Acenaphthene-dl0 20.56
Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 Benzoic acid, /-ethoxy- , ethyl este 194 C11H1403 023676-09-7 96
2 n-Octyl-4-hydroxybenzoate 250 C15H2203 001219-38-1 47
3 Benzoic acid, 2-hydroxy-, :hydrazide 152 C7H8N202 000936-02-7 43
4 ortho -Hydroxyp rop iophenone 150 C9H10O2 _______ 000610-99-1 43
Abundance Scan 1741 (21.029 min): 30641.D (-)
121
m/z 120.95 100.00%
5000 149
138 194
65
93 166
i 39 20.60 20.80 21.00 21.20 21.40
.
m/z-> 20
,1 .
i ■ ■ ■ ■ I1
40
594414748—
60
76
80
11 109 I 179
■ ■ । ■ ■ ■ ■ । ' ■ ■ • । 1 ‘ ■ ■ । ■ ‘
100 120 140 160 180 200 220 240
m/z 149.00 47.49%
Abundance #21260: Benzoic acid, 4-ethoxy-, ethyl ester
121
149
5000
20.60 20.80 21.00 21.20 21.40
138 194
65 93 166 m/z 194.0,5 29.33%
27
।
i I ' ' ' 1 1 ' ' ' ' I ' ' ' 1 I ' t+t
m/z-> 20 40 60 80 100 120 140 160 180 200 220 240
Abundance *3937: n-Octyl-4-hvdrexybenzoate
121
20.60 20.80 21.00 21.20 21.40
5000 70 m/z 138.05 27.01%
138
93
56 ;
1 ! 250
i ' ' ■ ' i ' ' ' ' i ' ' ' ' I ' ' 1 1 i ' 1 ' ‘ I ■ ' ' 1 i 1 1 1 1 I ■ ' 1 ■ i ' ■ ■ ■ i ■ ' ' 1 i ■ ' ' ■ i 1 ' ' 1
• m/z-> 20 40 60 80 100 120 140___ 160 180 200 220 240
Abundance #10124: Benzoic acid, 2-hydroxy-, hydrazide — P—TP 1* 1pm । । । , .
121 20.60 20.80 21.00 21.20 21.40
m/z 64.9,5 21.61%
5000
65 93 152
53 |
i ■ ■ ■ ■ i ' 1 —P
37 —PPmTemmn
160 180 200 220 ' 240
miz-> 20 40 60 80 100 120 140 20.60 20.80 21.00 21.20 21.40
30641.D GCMS1126.M Mon Jan 28 11:14:05 2002 Page 6
NYC-WTC_000004420
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