Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
NYC-WTC_000036162–000036183Folder label: “GCMS X 12/3/01 A 12/10/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2 701\29231.D Vial: 57 Acq On : 30 Dec 2001 3:05 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Library C: \DATABASE\NBS75K . L ********************************************************************* Peak Number 8 Benzoic acid, 4-ethoxy-, ethyl Concentration Rank 9
R.T. EstConc Area Relative to ISTD R.T.
21.02 0.70 ug/1 939946 Acenaphthene -dl0 20.57
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Benzoic acid, 4-ethoxy-, ethyl este 194 C11H1403 023676-09-7 96 2 Anisyl propionate 194 C11H1403 007549-33-9 43 3 Benzoic acid, 2-hydroxy-, hydrazide 152 C7H8N202 000936-02-7 43 4 ortho-Hydroxypropiophenone 150 C9H10O2 000610-99-1 43 Abundance Scan 1741 (21.025 min): 29231.D (-) 121 m/z U 100.00% 5000- 149
138 194 65 93 ITT ' ' i ■ ■ ' ■ i ' ' ' ' i ' ' ' ■ i ' ■ ; 39 166 20.60 20.80 21.00 21.20 21.40 I m/z—> 30 — „ 50, ,, l ।, a , ++1Q9 40 50 60 76 U +158..179 70 80 90 100 110 120 130 140 150 160 170 180 190 200 m/z 14 9.00 48.10% Abundance #69400: Benzoic acid, 4-ethoxy-, ethyl ester 121
149 5000- 194 20.60 20.80 21.00 21.20 21.40 65 138 93 166 m/z 194.05 29.11% ! m/z-> 30 40 50 50 , 76 • i ■ ■" i'" ' i' 60 70 80 4 r I I. — 90 100 1W 120 130 140 150 160 170 180 190 200 Abundance I #21256; Anisyl propionate I 121 II 20.60 20.80 21.00 21.20 21.40 5000 m/z 138.05 25.72% 77 91 194 138 I 109 I TIT" ' i11' " ' I'' " i' ‘TTT ■' i' [ rmytm-]-Tn-ry r • ” r • • • i" • • i m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #10124: Benzoic acid, 2-hydroxy-, hydrazide 121 20.60 20.80 21.00 21.20 21.40 m/z 65.05 19.. 85% 5000
65' 93 152 37 53 -------------------- , - — I- ■ I'1 ■' i1 " ■ i'' “ i rr 11111111'" i1' " i' ■'' i■"' I "I’IIIT’ETTT "‘I‘IEIN‘‘"TT I " '' I m/z-> 30 40 50 60 70 80 90 100 119 120 130 140 150 160 170 180 190 200 20.60 20.80 21.00 21.20 21.40
29231 .D GCMS1126.M Mon Dec 31 13:59:39 2001 Page 8
NYC-WTC_000036175
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