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Document / 344 pages

DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004149–000004492

Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02

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Scanned page image, NYC-WTC_000004315
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search. Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30709.D Vial: 47 Acq On : 30 Dec 2001 4:24 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Benzoic acid, 4-ethoxy-, ethyl Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

21.02 1.96 ug/1 1254930 Acenaphthene-dl0 20.56

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzoic acid, 4-ethoxy-, ethyl este 194 C11H1403 023676-09-7 97 2 Ethylparaben 166 C9H10O3 000120-47-8 47 3 ortho-Hydroxypropiophenone 150 C9H10O2 000610-99-1 43 4 Benzpic acid, 2-hydroxy-, hydrazide 152 C7H8N202_______ 000936-02-7 43 Abundance ( Scan 1740 (21.018 mln): 30709.D (-) 121 " 120. s 100.00^ 5000 149

65 138 194 93 166 -----TTTT39 50 ,76 | 109 | 179 TTTICOOTTu 11 r 1 20.60 20.80 21.00 21.20 21.40 " " 47.96% m/z-> :20 30 40. 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200

d Abundance #21260: Benzoic acid, 4-ethoxy-, ethyl ester 121

149 5000 i > ■ > । i • • 138 20,60 20.80 21.00 21.20 21.40 194 27 65 93

m/z-> 1 ‘ r ■ ‘' i ■ “ ' i " " i' ■" i " " i' "' i' "L 11'11' ।1 ■ • ■ ।" I T’T 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 " i"

Abundance *13954. Ethylparaben 121

5000 " "s 26.33%^ 20.60 20.80 21.00 21.20 21.40

65 93 138 166 53 m/z-> :20 30 40 50 60 70 80 90'100 110 120 130 140 150 160 170 180 190 200 Abundance #9726: ortho-Hydroxypropiophenone 121 20.60 20.80 21.00 21.20 21.40 | m/ z 65.05 20.75% 5000

65 150 93

m/z-> 27 TPWTB)* 1 77 1 +131—7 i11" i" ■ ■ i11" r " ■ i " ‘' I ' ‘ " I " " i "11111" I "111" A-P-im T । r . > । r-r-r-T-f . i 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 20.60 20.80 21.00 21.20 21.40

30709.D GCMS1126.M Mon Jan 28 11:33:02 2002 Page 6

NYC-WTC_000004315

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NYC-WTC_000004315Source: NYC Law Department, mirrored locally

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