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GC/MS calibration data for sample 28322, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.

NYC-WTC_000018492–000018518

Folder label: “GCMS X 12/18/01 A 12/30/01

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Scanned page image, NYC-WTC_000018506
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\28322.D Vial: 62 Acq On : 30 Dec 2001 7:56 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Benzoic acid, 4-ethoxy-, ethyl Concentration Rank 15

R.T. EstConc Area Relative to ISTD R.T.

21.03 1.48 ug/1 731878 Acenaphthene-dl0 20.56

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Benzoic acid, 4-ethoxy-, ethyl este 194 C11H1403 023676-09-7 97 2 ortho-Hydroxypropiophenone 150 C9H10O2 000610-99-1 43 3 Benzoic acid, ethoxy-, ethyl ester 194 C11H1403 075333-22-1 43 4 Phenol, 4-fomylcarbonyl- 150 C8H603 _ 000000-00-0 43 Abundance Scan 1741 (21.028 min): 28322.D (-) m/z 120.90 100.00% 121

149 5000 138 194 65 93 166 20.60 20.80 21.00 21.20 2140 ' m/z-> 39 50 . mmpHmn 77 109 Tpmm il, ■•i•■• +179— 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 '11' ‘ m/z 149.00 4 9.70% Abundance #21260: Benzoic acid, 4-ethoxy-, ethyl ester 121

149 5000 138 194 20.60 20.80 21.00 21.20 21.40 65 93 166 m/z 194.0528.19% 27 1 1 l•“‘J•••H*‘ “I‘ ”I‘ " i' ■ m/z-> :20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundancei 40728 ortlHivdrosepmomophenone 121 1**I*’’’I**’I’ mr 20.60 20.80 21.00 21.20 21.40 5000- m/z "7 27.69% 65 150 93 27 77 i 131 ।.... 11111 p।11. i. ।।i1 • i'" ■ i “ ’ 1++++1++++1+***1**+*/** m/z-> : ■i •■ 20 30 i“ ■ ' i‘ 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #21246: Benzoic acid, ethoxy-, ethyl ester 121 20.60 20.80 21.00 21.20 21.40 m/z 64.9 19.98% 138 5000 194 29 65 149 | 39 93 166______ Ppo T‘—[B——2212232090000323317 ’IE"’I932111101-0 I I —1’1’12111911013772’11121331111135 111 “ 7 ‘ Oi .. is 1 miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 20.60 20.80 21.00 21.20 21.40

28322.D GCMS1126.M Wed Feb 06 12:56:18 2002 Page 9

NYC-WTC_000018506

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NYC-WTC_000018506Source: NYC Law Department, mirrored locally

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