Analytical notes regarding GCMS scan results and LCS standard recoveries for sample AD30986.
NYC-WTC_000018287–000018315Folder label: “GCMS X 12/27/01 A 1/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File C: \HPCHEM\ 1 \DATA\ JANI 802\30986A.D Vial: 3 Acq On 18 Jan 2002 5:36 pm Operator: 209 GALOS Sample Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 Benzoic acid, 4-ethoxy-, ethyl Concentration Rank 17 R.T. EstConc . Area Relative to ISTD R.T.
20.82 0.58 ug/1 294085 Acenaphthene-dl0 20.36
Hit# of 5 ntative ID MW MolForm CAS# Qual
1 Benzoic acid, 4-ethoxy-, ethyl este 194 C11H1403 023676-09-7 96 2 Benzoic acid,.ethoxy-, ethyl ester 194 C11H14O3 075333-22-1 43 3 Phenol, 4-fomylcarbonyl- 150 C8H603 000000-00-0 43 4 1-Pentanone, 1-(4-hydroxyphenyl)- 178 C11H1402 002589-71-1 43 Abundance Scan 1718 (20.818 min): 30986A.D (-) I m/z 120.9.5 100.00% 121
5000 149 138 194 39 65 93 166 I 1 1 I 1 1 1 TIT-ps 1 ■ । ’ 20.40 20.60 20.80 21.00 21.20 i m/z~> I 50 76 . 109 0- 11111 1 11 1 i I} r’i r’t’r 11 i'It. । rrl’r’ni 11 All . 1 .‘I r >... । :20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 I i, I 179 t... . |... 111. r. ।.... ।.... ]. ‘ .‘T m/z 149.0,0 47.58% Abundance* #21260: Benzoic acid, 4-ethoxy-, ethyl ester 121
149 5000 /***t***.***14 138 20.40 20.60 20.80 21.00 21.20 194 65 93 166 m/z 194.05 27.79% 27 I TIp—Hpu ■ ■ i" m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #21248: Benzoic acid, ethoxy-, ethyl oster : 121 ...... R...... 20.40 20.60 20.80 21.00 21.20 138 m/z 138.05 27.05% 5000 194 29 65 149 | 39 93 166 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #9646: Phenol, 4-fomylcarbonyl- 121 20.40 20.60 20.80 21.00 21.20 m/z 64.95 20.93% 5000
65 93
m/z-> 46 TIWTTRTtgo 1221170011/0111/011170111/0111/
20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 I 150 'I . . . । l . . . ( . . . . | . . . . | > . . . । . . . . । . . 1 . । b . . . ! . . A. 20.40 20.60 20.80 21.00 21.20
30986A.D GCMS1126.M Tue Jan 22 10:18:12 2002 Page 11
NYC-WTC_000018305
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NYC-WTC_000018492
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018519
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018470
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033974
Laboratory report documenting GCMS analysis for unknown compounds and surrogate recovery in sample AD28335 conducted on January 9, 2002.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036614
Laboratory comments on GCMS scan results for sample AD29466 noting low recovery and scheduling re-extraction.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · similarity 0.996
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NYC-WTC_000018058
Document with unreadable text from the GCMS X folder series in DEP Box 16.
Filed in the same folder
NYC-WTC_000018059
Calibration verification report using DFTPP standard for GCMS instrument performance check on January 1, 2002.
Filed in the same folder
NYC-WTC_000018060
Laboratory report documenting GCMS calibration analysis of sample AD30694 conducted on January 18, 2002.
Filed in the same folder
NYC-WTC_000018064
Reference data table listing response factors and concentrations for organic compounds used in GCMS analysis of sample AD30694.
Filed in the same folder
NYC-WTC_000018069
Blank analysis report showing non-detectable levels of target organic compounds in sample AD30694.
Filed in the same folder