GC/MS calibration data for sample 30647, Dec 2001

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Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.

NYC-WTC_000018546–000018575

Folder label: “GCMS X 12/18/01 A 12/30/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC2701\30706.D Vial: 54 Acq On : 30 Dec 2001 12:10 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Benzoic acid, 4-ethoxy-, ethyl Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

21.03 1.10 ug/1 611783 Acenaphthene-dl0 20.57

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Benzoic acid, 4-ethoxy-, ethyl este 194 C11H1403 023676-09-7 96 2 Ethylparaben 166 C9H10O3 000120-47-8 53 3 Benzenepropanoic acid, 4-methoxy-, 194 C11H14O3 015823-04-8 43 4 1-Pentanone, 1- (4-hydroxyphenyl) - 178 C11H1402: 002589-71-1 38 Abundance Scan 1742 (21.034 mln): 30706.D (-) m/z 120.95 100.00% 121

149 5000 138 194 65 93 • 1 t ' • 1 1 I ' 1 1 1 I 1 1 166 0 mmptmt 39 50 , —mmmmor iremm 76 os J 109 | ■i ।.»। . j... j । j H i p i 179 20.80 21.00 21.20 21.40 m/z 149.00 51.21% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #21260: Benzoic acid, 4-ethoxy-, ethyl ester 121

149 5000 138 194 20.80 21.00 21.20 21.40 ' 65 93 166 I m/z 194.05 29.26% 27 1 Tp 1’’1’***I*4* ।.... 11 ‘ ‘l‘*A+AAAIA‘‘‘I" "i" miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundant® #13954, Ethylparaben 121 T TPTTT 20.80 21.00 21.20 21.40 5000 m/z 138.05 28.37% 65 93 138 166 53 ■I “'“i ““i t। f.... । m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #21262: Benzenepropanoic acid, 4-methoxy-, methyl ester 121 20.80 21.00 21.20 21.40 m/z 64.95 20.40% 5000 194 134 108 . I, 151 163 ... (. I. . t.... j.... । }.... j....,. ’ I’ opnaprho i i i ( । i ippom j 7 11' m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 20.80 21.00 21.20 21.40

30706.D GCMS1126.M Fri Feb 01 11:08:20 2002 Page 7

NYC-WTC_000018567

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