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Document / 344 pages

DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004149–000004492

Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02

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Scanned page image, NYC-WTC_000004449
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2 701\30707.D Vial: 41 Acq On : 29 Dec 2001 10:35 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Benzoic acid, 4-ethoxy-, ethyl Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

21.03 1.16 ug/1 675661 Acenaphthene-dl0 20.56

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzoic acid, 4-ethoxy-, ethyl este 194 C11H1403 023676-09-7 97 2 Ethylparaben 166 C9H10O3 000120-47-8 60 3 Benzenepropanoic acid, 4-methoxy-, 194 C11H14O3 015823-04-8 43 4 1-Cyclopfentene-1-propanoic acid, .b 168 C10H16O2___ _ 061833-30-5 42 Abundance Scan 1741 (21.030 min): 30707.D (-) m/z 120.95 ”100.00% 121

149 5000 138 194 65 1 1 1 1 1 I 1 1 1 1 I ' 1 ' ' i ' ' ' ' 1 1 1 93 166 39 50 TTThhmtnm mpHm h 77 J 109 JU .... ....... . 20.60 20.80 21.00 21.20 21.40 m/z 149.00 51.40% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #21260: Benzoic acid, 4-ethoxy-, ethyl ester ; 121

149 5000- _ ..... P— , , . . , 1 20.60 20.80 21.00 21.20 21.40 138 194 65 93 166 m/z 194.05 28.47% 27 I 11’111100110100110011001011 —7031" " ■ i"" 11" " I" " l"1'' i11 - ‘ I’’ m/Z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance 13954. Ethylparaben 121 i ■ ■ ■ ■ i ■ ■ - • j • ■ 1 ' l 1 ' TT T ' 20.60 20.80 21,00 21.20 21.40 5000 m/z 138.05 26.27% 65 93 138 166 53 m/z-> :20 30 40 50 60 70r' "80i" ■90r i1 ■"100i ‘1 ■110 ' i " " i" " i i' “ ‘ i " ■' ■ i ■ ■'11 ■ ■ ■ ■ i “'11" ■ ■ i' "' r " ' r ■'1 r "1 r'1' i" 120 130 140 150 160 170 180 190 200 Abundance #21262: Benzenepropanoic acid, 4-methoxy-, methyl ester ------ 121 20,60 20.80 21.00 21.20 21.40 m/ z 64.9.5 20.44% 5000 194 134

miz-> ■ i > ■ > • i ■ > ■ ■ i ■ ■ >' i1 ‘1 ■ i ■ ■' • i ■ ! ■ ■' I LU 108 151 163 i ‘" i' " ' r'1" i " " r " ' r " l" 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 20.60 20.80 21.00 21.20 21.40 TPTr ■ ■ i 1 ■ ■ ’ i ■ TPTT

30707.D GCMS1126.M Mon Jan 28 11:24:11 2002 Page 7

NYC-WTC_000004449

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NYC-WTC_000004449Source: NYC Law Department, mirrored locally

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