Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
NYC-WTC_000004149–000004492Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2 701\30707.D Vial: 41 Acq On : 29 Dec 2001 10:35 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 8 N-(Trifluoroacetyl)-0,01,011-t Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T.
22.79 4.05 ug/1 2599330 Phenanthrene-dl0 24.99
Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 N-(Trifluoroac yl)-0,0',0''-tris(t 481 C19H34F3NO4Si3 000000-00-0 35 2 Benzoic acid, ■ 2,6-bis[(trimethylsil 370 C16H30O4Si3 003782-85-2 32 3 Benzeneethanamine, N- [ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 25 4N-(Trifluora/etyl)-0,0',0"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 25 Abundance Scan 1933 (22.793 min): 30707.D (-) m/z 72.95 “ 100.00% 73
5000 147 355 221 281 j 22.40 22.60 22.80 23.00 23.20 J 45 ' ■ i '' ' — 117 191, 1.249, I, 327, 1 , 401 441 ........... , m/z 355.05 29.33% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58326: N-(Trifluoroacetyl)-O,O',6"-tris(trimethylsilyl)no 73 355 ........ .............. 5000 22.40 22.60 22.80 23.00 23.20 45 m/z 147.00 27.58% ! 120147 193 265 481 Tbil m/z- > 50 100 150 200 250 300 350 400 450 500 550 Abundance 451298. He azoic acd, 2.6-bis[(trimethyisilyi)oxy]-. trimet 73 355
22.40 22.60 22.80 23.00 23.20 5000 m/ z 221.05 19.89% 147 267 । 47 208 237 j....... |............. m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methylene] 73 355 22.40 22.60 22.80 23.00 23.20 m/ z 281.00 15.83% 5000
45 _ J , II, , 208 251 281 386 458 548 - m/z-> 50 100 150 200 250 300 350 400 450 500 550 22.40 22.60 22.80 23.00 23.20
30707.D GCMS1126.M Mon Jan 28 11:24:16 2002 Page 8
NYC-WTC_000004450
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28479 analyzed in early December 2001.
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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
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Analytical commentary for sample AD28149 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
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NYC-WTC_000004148
Fragmented OCR text showing dates and identifiers for a DEP GCMS record dated February 2002.
Filed in the same folder
NYC-WTC_000036712
GCMS analysis report for sample AD29563 listing unknown compounds and surrogate recovery data from January 28, 2002.
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