Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
NYC-WTC_000017833–000017853Folder label: “GCMS X 12/13/01 A 12/27/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC2701\30351.D Vial: 20 Acq On : 28 Dec 2001 6:36 am Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 N-(Trifluoracetyl)-0,0',0"-tri Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 22.79 2.86 ug/1 1170800 Phenanthrene-dl0 24.98 Hit# of 5 Tentative ID MW MolForm CAS# Qual
I N-(Trifluoracetyl)-0,0',0”-tris(tri 495 C20H36F3NO4Si3 000000-00-0 43 2 Benzeneethanamine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 43 3 N-(Trifluoroacetyl)-N,O,O ‘,011-tetr 553 C22H42F3NO4Si4 000000-00-0 35 4 Benzoic acid, Abundance 2,5-bis(trimethylsilo370C16H3004Si3 003618-20-0 28 Scan 1933 (22.788 min): 30351.D (-) m/ z 72.9.5 100.00% 73
5000 147 355 221 281
miz-> 45 117 191. | 249 L ' 1 111 + 1 TTPo 1 fiPi ri4 Pin r4 i 50 100 150 3?7 200 250 300 :350 Qz 22.40 22.60 22.80 23.00 23.20 400 450 500 550 m/z 147.00 26.95% Abundance #58807: N-(Trifluoracetyl)-O,O',O*-tris(trimethylsilyl)epin 73 355 5000 22.40 22.60 22*80 23.00 23.20 45 m/z 355.05 25.94% | + 140 184 281 480 * •'11 ‘ ■ 1 r i ■ ■ • ■ i • IIAIIIIITII-II1’’ >1' i'' ' ■ i' ■ miz-s 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-liperitafluorophenyh)methylene] 73 355 22.40 22.60 22.80 23.00 23.20 5000 m/z 221.05 18.24%
45 208 251 281 386 458 548 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60162: N-(Trifluoroacety!)-N,O,O’,O"-tetrakis(trimethylsi 73 22.40 22.60 22.80 23.00 23.20 m/z 281.00 14.70% 355 5000
I 45 — ■ ' i ■ ■ ■ 147 193 267 538 • 'i ■ ■ ■ 1 i ■ • ■ 1 i 1 ■' r ' TO3BnnmTOnCETT1133 miz-> 50 100 150 200 250 300 350 400 450 500 550 22.40 22.60 22.80 23.00 23.20
30351.D GCMS1126.M Wed Jan 02 10:46:21 2002 Page 6
NYC-WTC_0000 17845
OCR can misread numbers and units. Confirm readings against the page image before using them.
Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017724
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30426 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017808
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30352 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017675
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30251 conducted on January 9, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018546
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018470
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036712
GCMS analysis report for sample AD29563 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036798
GCMS analysis report for sample AD29523 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
Page similarity is temporarily unavailable or this page has no indexed vector.
Readers open these alongside this record — through an Ask answer, the same folder, or indexed similarity. Not a claim they are about the same event.
NYC-WTC_000017649
Single-page document containing GCMS data or metadata associated with the WTC site in December 2001.
Filed in the same folder
NYC-WTC_000017650
Laboratory log recording extraction parameters and sample counts for environmental samples processed in December 2001.
Filed in the same folder
NYC-WTC_000017654
Document showing calibration results for GCMS analysis of volatile organic compounds on December 27, 2001.
Filed in the same folder
NYC-WTC_000017658
Laboratory report documenting gas chromatography-mass spectrometry reference material analysis conducted on December 31, 2001.
Filed in the same folder
NYC-WTC_000017663
Laboratory report documenting gas chromatography-mass spectrometry blank analysis conducted on December 27, 2001.
Filed in the same folder