NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2701\30351.D Vial: 20
Acq On : 28 Dec 2001 6:36 am Operator: 209 GALOS
Sample : GC/MS SCAN 12/13 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
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Peak Number 7 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 8
R.T. EstCono Area Relative to ISTD R.T.
26.89 1.75 ug/1 713649 Phenanthrene-dl0 24.98
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 40
2 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 36
3 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 35
4 1-Monolinoleoylglycerol trimethylsi 498 C27H54O4Si2 054284-45-6 25
Abundance Scan 2380 (26.892 min): 30351 .D (-) m/z 72.95 100.00%
73
5000
147
221 281
26.60 26.80 27.00 27.20
45
1 114 1 ,.17, . ■ 1911 .2 1 24944 327,325 401 429 .............. m/z 147.00 34.03%
miz-> 50 100 150 200 250 350
300 400 450 500 550
Abundance #60503:3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim
73
5000 ‘ • i ‘ ' ' ■ i 1 ‘
147 26.60 26.80 27.00 27.20
221 281 327 m/z 281.00 19.22%
415 519 561
m/z-> 50 100 150 200 250 300 350 400 450 500 550
Abundance 52459 Trisilovane 1,1 1,5.5,5-hexamethyl-3,3-bis/(trimet
73 147
281 26.60 26.80 27.00 27.20
5000 m/z 221.05 17.16%
207 369
’*!1*’*I**1*+’*I’’ 29 338
miz-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #56714:1,1,1,5.7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t
73 26.60 26.80 27.00 27.20
m/z 74.00 8.17%
147
5000 267
355 429
45 207
t-» f ri . » । i i r i । > i j i । । ( । । [88 ■ ■ । ■ ■ • ■ । ' r-11 ■ ■ । ■
m/z-> 50 100 150 200 250 300 350 400 450 500 550 26.60 26.80 27.00 27.20
30351.D GCMS1126.M Wed Jan 02 10:46:26 2002 Page 7
NYC-WTC_000017846
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