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GCMS analysis results for sample AD30351, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.

NYC-WTC_000017833–000017853

Folder label: “GCMS X 12/13/01 A 12/27/01

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Scanned page image, NYC-WTC_000017846
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30351.D Vial: 20 Acq On : 28 Dec 2001 6:36 am Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 8

R.T. EstCono Area Relative to ISTD R.T.

26.89 1.75 ug/1 713649 Phenanthrene-dl0 24.98

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 40 2 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 36 3 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 35 4 1-Monolinoleoylglycerol trimethylsi 498 C27H54O4Si2 054284-45-6 25 Abundance Scan 2380 (26.892 min): 30351 .D (-) m/z 72.95 100.00% 73

5000 147 221 281 26.60 26.80 27.00 27.20 45 1 114 1 ,.17, . ■ 1911 .2 1 24944 327,325 401 429 .............. m/z 147.00 34.03% miz-> 50 100 150 200 250 350 300 400 450 500 550 Abundance #60503:3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73

5000 ‘ • i ‘ ' ' ■ i 1 ‘ 147 26.60 26.80 27.00 27.20 221 281 327 m/z 281.00 19.22% 415 519 561 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance 52459 Trisilovane 1,1 1,5.5,5-hexamethyl-3,3-bis/(trimet 73 147

281 26.60 26.80 27.00 27.20 5000 m/z 221.05 17.16%

207 369 ’*!1*’*I**1*+’*I’’ 29 338 miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #56714:1,1,1,5.7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t 73 26.60 26.80 27.00 27.20 m/z 74.00 8.17% 147 5000 267 355 429 45 207 t-» f ri . » । i i r i । > i j i । । ( । । [88 ■ ■ । ■ ■ • ■ । ' r-11 ■ ■ । ■ m/z-> 50 100 150 200 250 300 350 400 450 500 550 26.60 26.80 27.00 27.20

30351.D GCMS1126.M Wed Jan 02 10:46:26 2002 Page 7

NYC-WTC_000017846

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NYC-WTC_000017846Source: NYC Law Department, mirrored locally

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