NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2 701\30425.D Vial: 5
Acq On : 27 Dec 2001 3:04 pm Operator: 209 GALOS
Sample : GC/MS SCAN 12/13 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 8 3-Isopropoxy-l, 1,1,7,7,7-hexam Concentration Rank 6
R.T. EstConc Area Relative to ISTD R.T.
26.89 1.24 ug/1 523148 Phenanthrene-dl0 24.98
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 45
2 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 36
3 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 36
4 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 32
Abundance Scan 2380 (26.891 min): 30425.D (-) m/ z 73.00 100.00%
73
5000
147
221 281
327 355 399 429 26.60 26.80 27.00 27.20
TfT , , 191, [249 ’II I*I1*———*BmmWWTTT
45 117
TT TIPIT-C m/z 147.00 34.28%
m/z~> 50 100 150 200 250 300 350 400 450 500 550
Abundance #60503:3-lsoprapoxy-1,1,1,7,7,7-hexamethyl-3,5,5-trls(trim
73
5000-
147 26.60 26.80 27.00 27.20
ii m/z 281.00 18.37%
221 281 327 415
1 1 1. 519 561
miz-> 50 ' 100 ' 150 ' ‘ 200 250 300 " 350 ' 400 “ 450 ' ‘ 500 ' 550 '
Abundance #58871:1 -Monolinoleoylglycercl trimethylsily ether
73
207 26.60 26.80 27.00 27.20
5000 147 m/z 221.05 16.93%
34 103
281
395 482
■ ■ i ■ 1 ■ ■ i ‘ • ■ ■ i • 1 ■ 1 i ' ■ ■ ' i ‘ • i ■ • ■ ■ i • ■ ■ ' i ■ 1 ■ ■ i ' ■
m/z-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet
73 147 26.60 26.80 27.00 27.20
281
m/z 74.00 8.30%
5000
207 369
m/z—>
—— —
50 100 150
.2291.38
200 250 300 350 400 450 500 550
-----
26.60 26.80 27.00 27.20
30425.D GCMS1126.M Wed Jan 02 11:04:14 2002 Page 8
NYC-WTC_000017717
OCR can misread numbers and units. Confirm readings against the page image before using them.