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GCMS analysis results for sample AD30425, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.

NYC-WTC_000017703–000017723

Folder label: “GCMS X 12/13/01 A 12/27/01

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Scanned page image, NYC-WTC_000017717
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2 701\30425.D Vial: 5 Acq On : 27 Dec 2001 3:04 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 3-Isopropoxy-l, 1,1,7,7,7-hexam Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

26.89 1.24 ug/1 523148 Phenanthrene-dl0 24.98

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 45 2 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 36 3 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 36 4 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 32 Abundance Scan 2380 (26.891 min): 30425.D (-) m/ z 73.00 100.00% 73

5000 147 221 281 327 355 399 429 26.60 26.80 27.00 27.20 TfT , , 191, [249 ’II I*I1*———*BmmWWTTT 45 117 TT TIPIT-C m/z 147.00 34.28% m/z~> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503:3-lsoprapoxy-1,1,1,7,7,7-hexamethyl-3,5,5-trls(trim 73

5000- 147 26.60 26.80 27.00 27.20 ii m/z 281.00 18.37% 221 281 327 415 1 1 1. 519 561 miz-> 50 ' 100 ' 150 ' ‘ 200 250 300 " 350 ' 400 “ 450 ' ‘ 500 ' 550 ' Abundance #58871:1 -Monolinoleoylglycercl trimethylsily ether 73

207 26.60 26.80 27.00 27.20 5000 147 m/z 221.05 16.93% 34 103 281 395 482 ■ ■ i ■ 1 ■ ■ i ‘ • ■ ■ i • 1 ■ 1 i ' ■ ■ ' i ‘ • i ■ • ■ ■ i • ■ ■ ' i ■ 1 ■ ■ i ' ■ m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147 26.60 26.80 27.00 27.20 281 m/z 74.00 8.30% 5000

207 369

m/z—> —— — 50 100 150 .2291.38 200 250 300 350 400 450 500 550 ----- 26.60 26.80 27.00 27.20

30425.D GCMS1126.M Wed Jan 02 11:04:14 2002 Page 8

NYC-WTC_000017717

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NYC-WTC_000017717Source: NYC Law Department, mirrored locally

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