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GCMS analysis results for sample AD30425, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.

NYC-WTC_000017703–000017723

Folder label: “GCMS X 12/13/01 A 12/27/01

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Scanned page image, NYC-WTC_000017718
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30425.D Vial: 5 Acq On : 27 Dec 2001 3:04 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 1-Monolinoleoylglycerol trimet Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

28.65 0.99 ug/1 419017 Phenanthrene-dl0 24.98

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1-Monoliholeoylglycerol trimethylsi 498 C27H54O4Si2 054284-45-6 38 2 Benzeneethanamine, N-[ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 37 3 N-Methyladrenaline, tri-TMS 413 C19H39N03Si3 000000-00-0 28 4 Benzoic acid, 2f4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 25 Abundance Scan 2572 (28.654 min): 30425.D (-) m/z 73.0,0 100.00% 73

5000

45 1 ■ "I 1 1 ■-■■I 117*— 147 221 281 355 1911 I 249, I.-. 327, 4 401 429 ............... • ‘ i ' A 1 'l ‘ ‘ ' 1 l ' ' 28.40 28.60 28.80 29.00 m/z 147.00 34.26% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58871:1-Monol inoleoylglycerol trimethylsilyl ether 73

207 5000 147 28.40 28.60 28.80 29.00 34 103 m/z 355.05 19.27% 281

50 100 150 ‘ ‘ 200 250 I i , 3y, .482 300 ‘ ‘ 350 ' ' 400 450 500 550 miz-> Abundance #74706; Benzeneethanamine, N-Kpentafluorophenyl)methylenc] 73 355 dmn//n/m//nno/n/m 28.40 28.60 28.80 29.00 5000 m/z 221.05 18.54%

45 208 251 281 388 458 548 * * i ■ ’ ■ 1 i 1 1 • ■ I ■ ’ 1 1 i ■ ‘ ' i ‘ TPT / 1 11′4′8′4 r-1 *1***‘1** m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #54808: N-Methyladrenaline, tri-TMS 73 28.40 28.60 28.80 29.00 m/z 281.00 14.76% 5000 355 45 207 267 323 1 , , ।r. . । > 11 ■ । । i i । । *i > ■ i ] । -------------------- m/z-> 50 100 150 200 250 300 350 400 450 500 550 28.40 28.60 28.80 29.00

30425.D GCMS1126.M Wed Jan 02 11:04:19 2002 Page 9

NYC-WTC_000017718

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NYC-WTC_000017718Source: NYC Law Department, mirrored locally

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