NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2 701\30425.D Vial: 5
Acq On : 27 Dec 2001 3:04 pm Operator: 209 GALOS
Sample : GC/MS SCAN 12/13 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 10 1-Monolinoleoylglycerol trimet Concentration Rank 7
R.T. EstConc Area Relative to ISTD R.T.
30.25 1.22 ug/1 340744 Chrysene-dl2 33.02
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1-Monol inoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 45
2 2-Hexenedioic acid, bis(trimethylsi 288 C12H2404Si2 055494-10-5 23
3 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 23
4 Ethanedioic acid, bis(trimethylsily 234 C8H1804Si2 018294-04-7 23
Abundance Scan 2746 (30.251 mln): 30425.D (-) m/z 73.0,0 100.00%
73
5000 147
221 281 355 429 1 1 । • ‘ 1 rr 1 1 ' । 1 1
30.00 30.20 30.40 30.60
45 94 117 , , 1911 .. 249,
TIT TI I < '■ Pi* ' 327, L t 4011 m/z 147.00 38.26%
m/z-> 50 100 150 200 250 300 350 400 450
Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether
73
207
5000 147 TTT d4*
30.00 30.20 30.40 30.60
34 103
281 m/z 221.05 20.74%
m/z->
1
50
i ■ ' ■ '
100
i '
150
• ■
200
■ i
250
■ ■ ■
300
■ i
350
• ■ '
400
■ i ‘ '
.....a
1 395
• । * < * >
450
482
Abundance #40/77. 2-Hexenedioic acid. bis(tnmethylsily!) ester, (E}-
73
30.00 30.20 30.40 30.60
5000 m/z 355.0 13.01%
147
45
i, 112 _______ 244 273__________________
■ t ■ 1
m/z-> 50 100 150 200 250 300 350 460' 450
Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylslloxy)t
73 30.00 30.20 30.40 30.60
m/z 281.00 12.93%
147
5000 267
355 429
m/z~>
■
45
* i
50
......
+1*1**
100
Il
150 200
207
1.... . 250 ‘ 300 ‘ 350 400 450
-
30.00 30.20 30.40 30.60
30425.D GCMS1126.M Wed Jan 02 11:04:23 2002 Page 10
NYC-WTC_000017719
OCR can misread numbers and units. Confirm readings against the page image before using them.