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GCMS analysis results for sample AD30425, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.

NYC-WTC_000017703–000017723

Folder label: “GCMS X 12/13/01 A 12/27/01

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Scanned page image, NYC-WTC_000017719
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2 701\30425.D Vial: 5 Acq On : 27 Dec 2001 3:04 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 1-Monolinoleoylglycerol trimet Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

30.25 1.22 ug/1 340744 Chrysene-dl2 33.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Monol inoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 45 2 2-Hexenedioic acid, bis(trimethylsi 288 C12H2404Si2 055494-10-5 23 3 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 23 4 Ethanedioic acid, bis(trimethylsily 234 C8H1804Si2 018294-04-7 23 Abundance Scan 2746 (30.251 mln): 30425.D (-) m/z 73.0,0 100.00% 73

5000 147 221 281 355 429 1 1 । • ‘ 1 rr 1 1 ' । 1 1 30.00 30.20 30.40 30.60 45 94 117 , , 1911 .. 249, TIT TI I < '■ Pi* ' 327, L t 4011 m/z 147.00 38.26% m/z-> 50 100 150 200 250 300 350 400 450 Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether 73

207 5000 147 TTT d4* 30.00 30.20 30.40 30.60 34 103 281 m/z 221.05 20.74%

m/z-> 1 50 i ■ ' ■ ' 100 i ' 150 • ■ 200 ■ i 250 ■ ■ ■ 300 ■ i 350 • ■ ' 400 ■ i ‘ ' .....a 1 395 • । * < * > 450 482

Abundance #40/77. 2-Hexenedioic acid. bis(tnmethylsily!) ester, (E}- 73

30.00 30.20 30.40 30.60 5000 m/z 355.0 13.01% 147 45

i, 112 _______ 244 273__________________ ■ t ■ 1 m/z-> 50 100 150 200 250 300 350 460' 450 Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylslloxy)t 73 30.00 30.20 30.40 30.60 m/z 281.00 12.93% 147 5000 267 355 429

m/z~> ■ 45 * i 50 ...... +1*1** 100 Il 150 200 207 1.... . 250 ‘ 300 ‘ 350 400 450 - 30.00 30.20 30.40 30.60

30425.D GCMS1126.M Wed Jan 02 11:04:23 2002 Page 10

NYC-WTC_000017719

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NYC-WTC_000017719Source: NYC Law Department, mirrored locally

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