GCMS calibration table for TCLP analysis, Nov 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\JAN0802\28327.D Vial: 5 Acq On 8 Jan 2002 4:16 pm Operator: 209 GALOS Sample 508 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 1-Monolinoleoylglycerol trimet Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

. 32.94 3.02 ug/1 1015960 Chrysene-dl2 32.85

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-MonolinoleoyWlycerol trimethylsi 498 C27H5404Si2 054284-45-6 45 2 3-Isopropoxy-Zl,l,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 42 3 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 32 4 2 -Hexenedioic acid, bi s (trimethylsi 2 8 8 C12H2404Si2 055494-10-5 23 Abundance Scan 3038 (32.937 min): 28327.D (-) m/z 100.00% 73

5000 147 221 281 355 1 ' l' ' । ' I ' 1 1 ' i

—117—1914— 249+1325.— 401 428 .......... 45 32.60 32.80 33.00 33.20 T.n t rn/z 147.00 44.40% m/z-> 50 ...100___150__ 200 250 300.. .350 400 450 500 550 Abundance #58871; 1-Monolinoleoylglycerol trimethylsilyl ether 73 *

207 5000 147 । M d ' ' ' In- r . . । . i . . । i i > i । 32.60 32.80 33.00 33.20 34 103 j 281 m/z 221.05 2 5.52% s 3?5 482 1 ■ i 1 ' 1 ' । 1 1 ‘ | • r « i f f i — — TIu—nmonnvr m/z—> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503. 3-iB0prpoxe;.: .1,7.7.7-hexamethyl-3,5,5-tris(trim 73

32.60 32.80 33.00 33.20 5000 m/z 281.00 15.70%

.. L . 147 221 281

m/z-> 50 100 150 200 250 300 227, 415 ■ . .... . ' 350 " 400 " 450 ' 500 550 '

i Abundance

5000 73 #71006: Ethanedioic acid, bis(trimethylsilyl) ester

147 m/z J 32.60 32.80 33.00 33.20 15.58%

45 190 219 I I 117 -h-mmpmmmmm miz-> 50 100 150 200 250 300 350 400 450 500 550 32.60 32.80 33.00 33.20

28327.D GCMS1126.M Wed Jan 09 09:15:40 2002 Page 13

NYC-WTC_000033930