GCMS analytical comments for sample AD30986, Jan 2002

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Library Search Compound Report

Data File C:\HPCHEM\1\DATA\JANI802\30986A.D Vial: 3 Acq On 18 Jan 2002 5:36 pm Operator: 209 GALOS Sample Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 16 1-Monolinoleoylglycerol trimet Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

31.53 1.65 ug/1 639635 Chrysene-dl2 32.81

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1 -Monol inoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 45 2 3 -Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 30 3 2-Hexenedioic acid, bis (trimethylsi 288 C12H24O4Si2 055494-10-5 23 4 2-Ethy]Z3-trimethylsilyloxy(trimeth 276 C12H2803Si2 000000-00-0 23 Abundance Scan 2885 (31.532 mln): 30986A.D (-) m/z 73.0,0 100.00% 73

5000 147 221 281 1 • i * 1 -r ।-| i-r । । i "TTu i 1T 355 290 31.20 31.40 31.60 31.80 445+ 117 2,11914+, 24944 327,3501 400 401 . ................... 450 500 550 m/z 147.00 41.40% miz-> 50 100 150 200 250 300 Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether 73 207 5000 147 • ■ i • • • • i ■ '1 ' 11 1111* I 31.20 31.40 31.60 31.80 34 103 i m/z 221.05 22.10% 281 I . , . . 395, ...482. miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-Isopropoxy-1 .1,1.7,7.7-hexamethy!-3,5,5-tris(trim 73 ■ ‘ i ' ■ ■ 1 i ‘ * i ' ' ' ■ i 31.20 31.40 31.60 31.80 5000 m/z 281.00 15.41% 147

221 281 327 415 519 561 > • 1 > i 11 1 1 i '' 1 1 i 1 1 ' 1 i FT-r 11’441/ m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #40777:2-Hexenedioic acid, bis(trimethylsilyl) ester, (E)- * i • • • * i 73 31.20 31.40 31.60 31.80 m/z 355.0 10.91% 5000 147 45 | 112 244 273 i ■ TTYr • ■ i ‘ i ■ ■ ■ ■ i ■ ■ 1 •' i ■ ■ ‘ ■ i ' 1 ■ • i • ‘ ' i ‘ ' i ‘ ' 1 1 i ■ ■ 1 • i 1 ' miz-> 50 100 150 200 250 300 350 400 450 500 550 31.20 31.40 31.60 31.80

30986A.D GCMS1126.M Tue Jan 22 10:18:35 2002 Page 16

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