GCMS unknowns analysis results for sample AD28335, Jan 2002

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN0802\28355A.D Vial: 4 Acq On : 8 Jan 2002 6:13 pm Operator: 209 GALOS Sample : Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 16 1-Monolinoleoylglycerol trimet Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

32.93 7.79 ug/1 2345280 Chrysene-dl2 32.84

Hit# of 5 Tentative ID MW MolForm CAS# Qual

l 1-Monolinoleoylglycerol trimethylsi 498 C27H54O4Si2 054284-45-6 45 2 3-isopropoxy-1, 1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 40 3 Ethanedioic Zeid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 32 _ 4 Butanoic acid. 3-methyl-2-[(trimeth 262 CllH26O3Si2 055124-92 -02 3 Abundance Scan 3038 (32.931 mln): 28355A.D (-) m/ z 73.00 100.00% 73

5000 147 221 281 355 32.60 32.80 33.00 33.20

m/z-> 0- T. T T r 50 45 100 117 Pr +1914—— 249. 327. ( . TT401 , । 1er 150 200 250 300 350 400 450 500_550 T 429. ,. T.TPTTITT. ,. ,. ,. r, m/z 147.00 45.11% Abundance #58871:1-Monoiinoieoylglycerol trimethyisilyl ether 73

207 5000 147 32.60 32.80 33.00 33.20____ 34 103 | m/z 221.05 2 7.01% 1 281 ■ ‘ t ’ » ‘ ' ' i ' ' ■ ' 111 . । । . . r. । i > । > i 395482 TITru’aTur miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503; 3-ssopropoxy- !. 1,1.7.7,7-hexamethyl-3,5,5-tris(trim 73 .... Tnr ' ' I ‘ 1 I 32.60 32.80 33.00 33.20 5000 m/z 281.00 16.54% 147 221 281 327 415 519 561 . ................................ , , . . . TTT. T TTT TT miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #71006: Ethanedioic acid, bis(trimethylsilyl) ester .................... ------- 73 32.60 32.80 33.00 33.20 j | m/z 355.05 15.68% 147 5000

45 190 219 J_ L 117 1 1 1 1 r1 1 1 1 TTT - — • i ■ • > • । । । l • • • । i • • ■ • i • • • ■ i • ' • < t • ■ ----- 11. PPP m/z-> 50 100 150 200 250 300 350 400 450 500 550 32.60 32.80 33.00 33.20

28355A.D GCMS1126.M Wed Jan 09 09:10:12 2002 Page 16

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