Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
NYC-WTC_000018470–000018491Folder label: “GCMS X 12/18/01 A 12/30/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC2701\30645.D Vial: 53 Acq On : 30 Dec 2001 10:14 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 1-Monolinoleoylglycerol trimet Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 31.71 1.81 ug/1 662836 Chrysene-dl2 33.03
Hit# of 5 Tentative- ID MW MolForm CAS# Qual 1 1 -Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 45 2 Ethanedidic acid, bis(trimethylsily 234 C8H18O4S12 018294-04-7 32 3 2-Hexenedioi a acid, bis (trimethylsi 288 C12H2404Si2 055494-10-5 23 4 Butanoic acid, 3-methyl-2-[(trimeth 262 CllH26O3Si2 055124-92-0 23 Abundance / Scan 2905 (31.714 mln): 30645.D (-) m/ z 73.00 1 00.00% 73
5000 147 221 • • i ■ ‘ ‘ • i T T 281 355 31.40 31.60 31.80 32.00
m/z~> „ 45 0 114 r ri -| 11 "I 50 96 117 . 100 +-,11914 150 200 — 2494 250 300 1**T 350 325 401 429 ■ T ri V । । । । 400 450 m/z 147.00 40.84% Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether 73
207 _____________ ) v_____________ 5000 147 1 1 i • ‘ • i • ■ ■ ■ I ■ • • • i ■ • ■ • i 31.40 31.60 31.80 32.00 34 103 m/z 221.05 23.09% 281 [ t 395 482 - m/Z-> 50 100 150 200 250 300 350 400 450 Abundance #71006: Ethanedioic acid, bis(trimethylsilyi) ester 73 147 3140 31.60 31.80 32.00 ‘ ' 5000 m/z 281.00 15.64% 45 : 117 190 219 • m/z-> 50 100 150 2W 250 300 350 400 450 Abundance #40777:2-Hexenedioic acid, bis(trimethylsilyl) ester, (E)- ■ ‘ i ‘ ‘ ■ i 73 31.40 31.60 31.80 32.00 1z 355." 10.75% 5000 147 45
m/z-> TTT 50 —12 100 150 1111111 200 244 273 250 300 350 I I * II I 400 450 « I । i > i • ।
31.40 31.60 31.80 32.00 i i i i ।~ i t < i । i i • i
30645.D GCMS1126.M Fri Feb 01 10:53:24 2002 Page 13
NYC-WTC_000018487
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NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018492
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018519
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017833
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017808
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30352 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017724
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30426 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
1 shared topics · similarity 0.997
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NYC-WTC_000018416
Single-page document containing GCMS data or metadata associated with the WTC site in December 2001.
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NYC-WTC_000018417
Laboratory log sheet detailing Method 508 extraction and analysis parameters for samples processed in December 2001.
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NYC-WTC_000018420
Laboratory report documenting GCMS blank analysis of sample AD30643 conducted on February 1, 2002.
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NYC-WTC_000018436
Laboratory report documenting GCMS calibration data for sample AD30643 conducted on February 1, 2002.
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NYC-WTC_000018440
Laboratory report documenting GCMS reference analysis of sample AD30643 conducted on February 1, 2002.
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