GCMS calibration table for TCLP analysis, Nov 2001

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Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.

NYC-WTC_000033911–000033935

Folder label: “GCMS X 11/20/01 A 11/26/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\JAN0802\28327.D Vial: 5 Acq On : 8 Jan 2002 4:16 pm Operator: 209 GALOS Sample : 508 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 1-Monolinoleoylglycerol trimet Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 31.56 3.02 ug/1 1015720 Chrysene-dl 2 32.85 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 45 2 3-Isopropoxy-1, 1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 40 3 Ethanedioic acid, bis (trimethylsily 234 C8H18O4Si2 018294-04-7 27 4 2-Hexenedi ic acid, bis(trimethylsi 288 C12H24O4Si2 055494-10-5 23 Abundance 7 Scan 2888 (31.560 min): 28327.D (-) m/z 73.00 100.00% 73

5000 147 .. —................ ............. ..................... 221 281

miz-s 45 TIT T 50 100 :? 117 r. *. TIT r 249, | , 150 191 200 250 300 327355 40142 m/z 147.00 350 400 450 500 550 ' 31.20 31.40 31.60 31.80 39.89% Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether 73

207 ................ — 5000 147 ) i । ■ j ' 31.20 31.40 31.60 31.80 34 103 ! m/z 221.0,5 22.33% _ T-r-p ’ , 1II........ 395.... 1482 ....... —BT TTTTTTTTTTT m/z-> 50 100 150 1200 250 300 350 400 450 500 550 Abundance #60503: 3-Isopropoxy-1.1.1,7.7,7-hexamethyl-3,5,5-tris(trim 73 1 I ' 1 ' T IT TOEErTT 31.20 31.40 31.60 31.80 5000 m/z 281.00 14.99% 147 221 281327 415 519 561 - 1*1nr-guuupDuuTT miz-> 50 100 ' 150 ’ 200 250 300~ 350 400 450 500 550 Abundance #71005: Ethanedioic acid, bis(trimethylsilyl) ester 73 31.20 31.40 31.60 31.80 1 m/z 355.05 10.63% 147 5000

45 117 190 219 “ * t 1 ' * * r * Wt T. '•>. T Tur 1. 11111. '. T .. 'I 11. 11 TTTPPT --PPP —PPPP. 1. ।. T miz-> 50 100 150 200 250 300 350 400 450 500 550 31.20 31.40 31.60 31.80

28327.D GCMS1126.M Wed Jan 09 09:15:35 2002 Page 12

NYC-WTC_000033929

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