GCMS analysis comments for sample AD29466 re-analysis required, Jan 2002

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Library Search Compound Report

Data File C: \HPCHEM\1\DATA\JAN0802\29466.D Vial: 6 Acq On 8 Jan 2002 5 :14 pm Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 1-Monolinoleoylglycerol trimet Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

31.56 19.75 ug/1 6376990 Chrysene-dl2 32.84

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 45 2 3-Isopropoxy- 1,1, 1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 42 3 Ethanedioic id, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 32 4 2-Hexenedioic acid, bis (trimethylsi 288 C12H2404Si2 055494-10-5 23 Abundance Scan 2888 (31.559 min): 29466.D (-) m/ z 73.00 100.00% 73

5000 147 221 281 355 31.20 3140 31.60 31.80 45 o- 1 ‘I ' 1 117 T—Pr TT 1914 249444 327. I 401 428 m/ z 147.00 43.02% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58871: 1-Monolino!eoylglycerol trimethylsilyl ether 73

207 5000 147 31.20 31.40 31.60 31.80 34 103 281 m/z 221.00 25.98% N m/z-> 50 100 150 200 250 — 300 350 — 325 .. ... ., 400 450 500550 Abundance #80503; 3-lsopropoxy-1,1,1.7.7.7-hexametliyl-3,5,5-tris(trim 73 J V 31.20 31.40 31.60 31.80 5000 m/z 281.10 16.82% 147

221 281 327 I 415 519 561 m/z-> 50 100 150 200 250 300 350 400450 500 550 Abundance #71006: Ethanedioic acid, bis(trimethylsilyl) ester ' I ' ' ' ‘ I ' ' 1 ■ l n ■ < > । > ■ ■' > । ■ 73 31.20 31.40 31.60 31.80 m/z 355.05 12.86% 147 5000

45 — I I 117 190 219 ■ ' i ' ■ ' I ’ ' ' I ' ' ' ’ I ' m/z-> 50 100 150 200 250 300 350 400 450 500 550 31.20 31.40 31.60 31.80

29466.D GCMS0103.M Wed Jan 09 16:16:54 2002 Page 13

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