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Document / 344 pages

DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004149–000004492

Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02

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Scanned page image, NYC-WTC_000004456
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30707.D Vial: 41 Acq On : 29 Dec 2001 10:35 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 14 1-Monolinoleoylglycerol trimet Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

34.37 1.66 ug/1 654393 Chrysene-dl2 33.03

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 1 054284-45-6 45 3-Isopropoxy-1/1,1,7,7,7-hexamethyl 576 C18H5207Si7 2 071579-69-6 40 3 Trisiloxane, 1, 1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 38 Ethanedioic acid, bis(trimethylsily 234 C8H1804Si2 4 018294-04-7 32 Abundance Scan 3194 (34.369 min): 30707.D (-) m/z 73

5000 147 221 281 355 1 i ' ■ ■ ■ I ■ 34.00 34.20 34.40 34.60 45 117 191 249 1 327, I , , 401 429 i hj FP— ' m/z 147.0,0 49.54% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58871:1-Monolinoleoylglycerol trimethylsilyl ether 73

207 5000 147 1 ■ I 1 34.00 34.20 34.40 34.60 34 103 | 281 m/z "7 27.45% ..... .... ........ . m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance q DOXy ■ 1 1.7.7.7-hexamethyls 5 5-tri (trim 73

34.00 34.20 34.40 34.60 5000 m/z 280.95 16.21% 147

m/z-> ...... 221./.201/.827....415.. 519.561 _ 50__ 100 150 200 250 300 350 400__ 450 500 550 Abundance #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet - T A Pro 1* 1 I ' ' TTTTTTf 73 34.00 34.20 34.40 34.60 147 m/z 355.05 14.55% 5000

m/z-> 45 ■ ‘ i '

50 ' 117 100 | 150 281

। ,297,249, ... J.......... 200 250 300 350 369

400 450 500 550 .... L • i 1 1 1 • i 1 34.00 34.20 34.40 34.60

30707.D GCMS1126.M Mon Jan 28 11:24:44 2002 Page 14

NYC-WTC_000004456

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NYC-WTC_000004456Source: NYC Law Department, mirrored locally

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