GCMS analysis results for sample AD30252, Jan 2002

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Data File : C:\HPCHEM\1\DATA\DEC2 701\30252.D Vial: 22 Acq On : 28 Dec 2001 9:31 am Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 1-Monolinoleoylglycerol trimet Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

33.09 4.08 ug/1 1115960 Chrysene-dl2 33.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 45 2 3-Isopropoxy-l,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 42 3 Ethanedioic acid, bis(trimethylsily 234 C8H1804Si2 018294-04-7 32 4 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 32 Abundance Scan 3055 (33.087 min): 30252.D (-) m/z 100.00% 73

5000 147 221 281 355 ■ 1 1 1 • 1 ‘ i 1 '

117 249.., 325, I 401 429 32.80 33.00 33.20 33.40 45 miz-> 0- ■ ''I 1 1 ■ ‘ i • IPr 50 100 150 200 1914——=f 250 11.k'i ' r r i* t 1 1m 300 350 400 450 500 550 m/z 147.00 48.63% Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether 73 207 5000 147 ■ • I 1 • 32.80 33.00 33.20 33.40 34 103 , 281 m/z 221.05 29.98%

miz-> • • i • • ■ • i » • ■ ■ i ‘ f ' ■ i ‘ f ‘ i ■ ■ ' ' i • ■ .395, ...482. 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-Isopropoxy-1.1.1 7.7,7-hexamethii 3.5,5-tris(trim 73 ------------------------ 32.80 33.00 33.20 33.40 5000 m/z 281.00 18.21% 147 221 281 327 415 519 561 ■ ■ i • ■ • ■ । ■ ■ ■ ■ ।1 ■ ‘ ‘ । •1 • • । ‘ । •' • ■ । ‘ । ■ ■ ■ ■ । • ■ ■ • । ■ ■ ■ • ।■ m/z-> 50 100 150 200 250, 300 350 400 450 500 550 Abundance #71006: Ethanedioic acid, bis(trimethylsilyl) ester TTI 1’4’7 TT tT’i ir I 73 32.80 33.00 33.20 33.40

A 18.13% 147 5000

45 I I 117 . 190200219 250 150 300 350 400 450 ' 500 ^6 ‘ ‘ l ' ' m/z-> 50 100 32.80 33.00 33.20 33.40

30252.D GCMS1126.M Wed Jan 02 10:42:54 2002 Page 12

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