GCMS analysis results for sample AD30352, Jan 2002

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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30352 conducted on January 10, 2002.

NYC-WTC_000017808–000017832

Folder label: “GCMS X 12/13/01 A 12/27/01”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30352.D Vial: 19 Acq On : 28 Dec 2001 5:38 am Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 1-Monolinoleoylglycerol trimet Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

31.72 2.44 ug/1 688873 Chrysene-dl2 33.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Monolinoleoylglycerol trimethylsi 498 C27H5404S12 054284-45-6 45 2 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 40 3 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 32 4 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 Abundance 73 Scan 2906 (31.719 min): 30352.D (-) m/z "T 018294-04-7 32

5000 147 221 45 117 1914 249 281 . 327, 355 [ 401 420 449 31.40 31.60 31.80 32.00 0- 1 1’13 ' Pr 1 1 ,5 Pih ■ 1 * |A 1 r i । i i 'i ■ i-i i i t |-■ m/z 147.00 41.35% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58871:1-Monolinoleoylglycerol trimethylsilyl ether 73

207 5000 147 31.40 31.60 31.80 32.00 34 103 , 281 m/z 221.05 23.91% ,i, 1, , i,i, , , , , II, ,, . ,i., /, , , , 395,.11482. 400 ' 450 500 550 m/z-> 50 100 150 200 250 300 350 Abundance #60503: 3-sopropoxy-1.1.1,7.7.7-hexamethyl-3,5,5-tris(trim 73 i II i j I 1 j n TT | “ I I J J T I I i " |1 31.40 31.60 31.80 32.00 5000 m/z 281.00 16.10% 147

221 281 327 415 519 561 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bisI(trimet 1 ■ i ' ■ ‘ 1 i 73 31.40 31.60 31.80 32.00 147 m/z 355.05 12.39% 5000 281 45 — 369 207 249 miz-> 50 —10012 ....................................... < l ■ 1 ■ 1 1 11 150 200 250 300 350 400 450 500 550 1 । . *14 T’ « i । » « r . । i t t J | i 4 . । । i । TTI—nmT 31.40 31.60 31.80 32.00

30352.D GCMS1126.M Wed Jan 02 10:51:08 2002 Page 13

NYC-WTC_000017828

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