NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2 701\30707.D Vial: 41
Acq On : 29 Dec 2001 10:35 pm Operator: 209 GALOS
Sample : GC/MS SCAN 12/18 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 11 1-Monolinoleoylglycerol trimet Concentration Rank 7
R.T. EstConc Area Relative to ISTD R.T.
30.25 2.50 ug/1 984004 Chrysene-dl2 33.03
Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 42
2 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 33
3 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H36O4Si5 003555-47-3 14
4 Benzoic acid. 2,6- bis[(trimethylsil 370 C16H30O4Si3 003782-85-2 11
Abundance ican 2745 (30.247 min): 30707.D (-) m/ z 73.00 100.00%
73
5000
147
221 281 355 1 ' I rT 1 1 I 1 ' 1 1 I 1 1
30.00 30.20 30.40 30.60
45 96 117
,y. 1911 L 249, 1,,, 327, J. 401 429
IIt+um m/z 147.0,0 36.58%
TT
m/z-> 50 100 150 200 250 300 350 400 450
[Abundance #58871:1-Monolinoleoylglycerol trimethylsilyl ether
73
207
5000 147 1 ■ । ■ ' ' ■ । ■ ■
30.00 30.20 30.40 30.60
34 22.03%
103
I 281 m/z 221.05
“T"
. .10. 395, 482
m/z-> 50 100 150 200 250 300 350 400 450
Abundance 56714 1.1 1 5.4. i H pt t < 1 । 1 i ir ch in it
73
■ ■ i ' ' ' i ' 1 ■ ■ i ' 1
147 30.00 30.20 30.40 30.60
5000 267 m/z 355.05 14.06%
355 429
45 । 207
m/z-> 50___ 100___ 150 200 250 __ 300___ 350__ 400 450
Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet
73 147 30.00 30.20 30.40 30.60
281
m/z 281.00 13.13%
5000
| 2ij)7 249
369
1 338 _
‘*1* ■ ■ i ' 1
m/z—> 50 100 150 200 250 300 350 400 450 30.00 30.20 30.40 30.60
30707.D GCMS1126.M Mon Jan 28 11:24:29 2002 Page 11
NYC-WTC_000004453
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