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GCMS analysis results for sample AD29523, Jan 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AD29523 listing unknown compounds and surrogate recovery data from January 28, 2002.

NYC-WTC_000036798–000036814

Folder label: “GCMS X 12/7/01 A 1/2/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\29523.D Vial: 37 Acq On : 29 Dec 2001 12:10 am Operator: 209 GALOS Sample : GC/MS SCAN 12/7 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 1-Monolinoleoylglycerol trimet Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

30.25 0.41 ug/1 184923 Chrysene-dl2 33.03

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Monolinoleoylglyce rol trimethylsi 498 C27H5404Si2 054284-45-6 36 2 1,1,1,5,7,7,7-Hept iethyl-3,3-bis (t 444 C13H40O5Si6 038147-00-1 23 3 Tris (trimethylsily 1)borate 278 C9H27BO3Si3 004325-85-3 12 4 Benzoic acid, ,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 12 •Abundance ' Scan 2746 (30.250 min): 29523.D (-) m/ z 73.00 100.00% 73

5000 147 221 k.■ • l k 1 •» ■ I ' • | 281 355 30.00 30.20 30.40 30.60 45 117 ... 429 I 1 I 1 1 f_ 191 . . 249 . . 327, J, 401 1 IT । * 1 । T 1 m/z 147.00 34.26% . m/z-> 50 100 150 200 250 300 350 400 450 'Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether 73

207 ... 5000- 147 30.00 30.20 30.40 30.60 34 103 । 281 m/z 221.05 21.14% I. 1 , II _ 305, . , . , , 482 m/z-> 50 100 150 200 250 300 350 400 450 Abundance #56714: 1,1.1.5,7.7.7-Heptainethyl-3.3-bis(trirnethylsiloxy)t 73 147 30.00 30.20 30.40 30.60 5000 267 m/z 281.00 13.63% 355 429 45 207 I I ...... .............. — I m/z-> 50 100 150 200 250 300 350 400 450 Abundance #39028: Tris(trimethylsilyl)borate / \ 73 221 30.00 30.20 30.40 30.60 m/z 355.05 11.74% 5000 263 133 175 ........... T m/z--> 50 100 150 200 250 300 350 400 450 30.00 30.20 30.40 30.60

29523.D GCMS1126.M Tue Jan 08 12:10:00 2002 Page 9

NYC-WTC_000036813

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NYC-WTC_000036813Source: NYC Law Department, mirrored locally

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