DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2 701\30708.D Vial: 49 Acq On : 30 Dec 2001 6:21 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 1-Monolinoleoylglycerol trimet Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

30.25 1.46 ug/1 612096 Chrysene-dl2 33.03

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 42 2 3-1sopropoxy ,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 38 3 1,1,1,5,7,7,' Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 23 4 Silanamine, 1 [2,6-dimethyl-4-[(tri 281 C14H27NOSi2 072088-09-6 22 Abundance ' Scan 2745 (30.246 min): 30708.D (-) m/ Z 73.0,0 ’ 100.00% 73

5000- 147 221

0- ■ 45 . 'i ■ ■ ,117.4 1911 1,249 281 325 [ 355 4012 m/z 147.00 ■ ■ l ■ I ■ ■ i ■ I । । । । I । । 30.00 30.20 30.40 30.60 35.50% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether 73

207 5000- 147 ■ ■ i t—«■ • r । । i । । ' ■ I 30.00 30.20 30.40 30.60 34 103 281 m/z 221.05 20.71%

m/z--> 1. . 395. 482 . 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503. 3-1s00!O0O*V-1 1 * 7.7.7-nawametny!-3,5,5-t 73 ■ I • ‘ 30.00 30.20 30.40 30.60 5000 12.80% 147 221 281 327 415 519 561 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiioxy)t ‘ ‘ ' I ' 1 1 ‘ f 1 ' 1 * i ■ ’ 73 30,00 30,20 30.40 30.60 m/z 281.00 12.15% 147 5000 267 355 429 207

m/z-> 45

50 100 150 200 I., 250 300 350 400 450 500 550 ' ' i 1 ' t*1 I 1 1 1 ' I ' ' 30.00 30.20 30.40 30.60

30708.D GCMS1126.M Mon Jan 28 11:29:08 2002 Page 12

NYC-WTC_000004351