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Document / 344 pages

DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004149–000004492

Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02

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Scanned page image, NYC-WTC_000004350
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2 701\30708.D Vial: 49 Acq On : 30 Dec 2001 6:21 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 3-Isopropoxy-l, 1,1,7,7,7-hexam Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

28.65 1.05 ug/1 685348 Phenanthrene-dl0 24.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Isopropoxy-4,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 40 2 Benzoic acid/ 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 37 3 1 -Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 33 4 1,1,1,5,7,7/7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 33 Abundance Scan 2571 (28.649 min): 30708.D (-) m/z 73.00 100.00% 73

5000 147 221 281 355 28.40 28.60 28.80 29.00 45. ' ''i ■ ■ 117 , , . 1914 [ । 249 . 327, 4 , , 401 429 m/z 147.00 34.52% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73

5000 147 28.40 28.60 28.80 29.00 221 m/z 221.05 18.91% I 281I 327 l i 415 519 561 m/z-> 50 100 150 200 250 300 350 400 450 500 550 ) Abundance #73975; Benzoic acid 2,4-bis[(trimethylsilyl)oxy]-, trimet 73

28.40 28.60 28.80 29.00 5000 355 m/z 355.05 16.45% 45 133 193 223 281

m/z-> 50__ 100__ 150 200 250 300 350 400 450 500 550 Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether ' 1 ■ ■ । ■ 1 1 ■ r1 1 ' I ' ' ‘ ' I ' ' 73 28.40 28.60 28.80 29.00 m/z 281.00 13.94% 207 5000 147 34 103

m/z-> 1 1 1 1 ' 1 ' 1 1 1 50 100 150 200 250 300 , । . 395, . 350 ,.482 400 450 500 550 28.40 28.60 28.80 29.00

30708.D GCMS1126.M Mon Jan 28 11:29:04 2002 Page 11

NYC-WTC_000004350

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NYC-WTC_000004350Source: NYC Law Department, mirrored locally

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