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GCMS analysis results for sample AD30252, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.

NYC-WTC_000017854–000017878

Folder label: “GCMS X 12/13/01 A 12/27/01

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Scanned page image, NYC-WTC_000017870
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC2701\30252.D Vial: 22 Acq On : 28 Dec 2001 9:31 am Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 1-Monolinoleoylglycerol trimet Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

28.65 2.21 ug/1 1106120 Phenanthrene-dl0 24.98

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 42 2 1,1,1,5,7,7,7-Heptamethy1-3,3-bis(t 444 C13H40O5Si6 038147-00-1 36 3 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207S17 071579-69-6 25 4 Benzoic acid. 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 25 Abundance Scan 2572 (28.653 min): 30252.D (-) m/z 73.0,0 100.00% 73

5000 147 221 281 355 28.40 28.60 28.80 29.00 45 r1 * 117 7.19111,249 ■. rI 1 . 327haast [ 401 429 sin . । । । 1 । m/z 147.00 35.26% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58871:1-Monolinoleoylglycerol trimethylsilyl ether 73

207 ____________ /____________ 5000 147 ***1**’’I*’’I’’I’*’ 28.40 28.60 28.80 29.00 34 103 m/z 221.05 19.66% 281 — ,.1.10. 300 482500 550 miz-> 50 100 150 ' 200 ‘‘ 250 350 400 450 Abundance #56714; 1.1. t .5.7.7.7-Heptametnyl-3.3-bis(trimethylsiloxy)t 73 .............. 7 V............ 147 28.40 28.60 28.80 29.00 1 5000 267 m/z 355.05 18.32% 355 429 45 207

m/z-> 50 100 150 200 250 300 350 400 450 ' 500 550 Abundance #60503:3-Isopropoxy-1,1,1,7.7,7-hexamethyl-3,5,5-tris(trim _ ------------ 73 28.40 28.60 28.80 29.00 m/z 281.00 15.09% 5000 147 221 281 327.... 415 059561 m/z-> 50 100 150 200 250 300 ' ' 350 ' 400 ‘ 450 500 550 28.40 28.60 28.80 29.00

30252.D GCMS1126.M Wed Jan 02 10:42:41 2002 Page 9

NYC-WTC_000017870

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NYC-WTC_000017870Source: NYC Law Department, mirrored locally

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