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GCMS analysis results for sample AD30426, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30426 conducted on January 10, 2002.

NYC-WTC_000017724–000017747

Folder label: “GCMS X 12/13/01 A 12/27/01

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Scanned page image, NYC-WTC_000017739
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30426.D Vial: 23 Acq On : 28 Dec 2001 11:28 am Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 l-Monolinoleoylglycerol trimet Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

28.65 1.48 ug/1 734867 Phenanthrene-dl0 24.98

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 l-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 34 2 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H52O7Si7 071579-69-6 25 3 Benzoic acid, 2,6-bis (trimethylsil 370 C16H30O4Si3 003782-85-2 14 4 Benzoic acid, 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 12 Abundance Scan 2572 (28.653 mln): 30426.D (-) m/z 73.0.0 100.00% 73

5000 147 221 281 355 28.40 28.60 28.80 29.00 m/z-> 45 • • •'i ' 50 117 100 +191+2494 1fr 150 200 250 300 350 400 450 500 550 327 1 401 429 tin mei fnt IIIII m/z 147.00 35.61% Abundance #58871: i-Monolinoleoylglycerol trimethylsilyl ether 73 ........ . ............ 207 5000 147 28.40 28.60 28.80 29.00 34 103 281 m/z 221.05 20.19% 395 482 i . miz-> 50 100 150 200 250 300 350 400 450 500 550 ' Abundance #60503: 3-Isopropoxy-1,1.1.7.7.7-hexamethy-3,5,5-tris(trim 73 — 28.40 28.60 28.80 29.00 5000 m/z 355.05 18.85% 147 221 281 327 415 519 561 171****1**‘‘I*‘**I**‘I‘**1******1***1 "TI * » i i । । । miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51296: Benzoic acid, 2,6-bis[(trimethylsilyl)oxy]-, trimet 73 355 2840 28.60 28*80 29.00 m/z 281.00 15.27% 5000-

147 267 47 208 237 | 1’1 * I u I 1 ' ' ■ i ‘ 1 1 1 i ' 1 ■ ■ i ■ ■ • • I ' 1 1 ' I 1 1 m/z-> 50 100 150 200 250 300 350 400 450 500 550 28.40 28.60 28.80 29.00

30426.D GCMS1126.M Wed Jan 02 11:08:11 2002 Page 8

NYC-WTC_000017739

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NYC-WTC_000017739Source: NYC Law Department, mirrored locally

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