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Document / 344 pages

DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004149–000004492

Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02

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Scanned page image, NYC-WTC_000004452
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC2701\30707.D Vial: 41 Acq On : 29 Dec 2001 10:35 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 1-Monolinoleoylglycerol trimet Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

28.65 1.68 ug/1 1078870 Phenanthrene-dl0 24.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Monolinoleoylglycerol trimethylsi 498 C27H54O4Si2 054284-45-6 42 2 Benzeneethanamine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 27 3 Benzoic acid, 2,A-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 25 4 3-1sopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 25 Abundance Scan 2571 (28.650 min): 30707.D (-) m/z 73.00 100.00% 73

5000 147 221 281 355 28.40 28.60 28.80 29.00 45 117. 191, . 249, [ 327 [ 401 429 .................... ' '11 1 1 m/z 147.00 34.60% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58871:1-Monolinoleoylglycerol trimethylsilyl ether 73

207 .................................. 5000 147 28.40 28.60 28.80 29.00 34 103 281 m/z 221.05 19.40% 395 _L I , 482 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance 5747061 Benzencethanamine N i nentefuorop"ci ymethylene] 73 355 28.40 28.60 28.80 29.00 5000 m/z 355.05 17.57%

45 : 208 251 281 386 458 548 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #73975: Benzoic acid, 2,4-bis[(trimethylsiiyl)oxy]-> trimet 73 28.40 28.60 28.80 29.00 m/z 281.00 14.28% 5000 355 45 133 193 223 281 . — 1 1 *_ —_ peger - l_ ------ m/z-> 50 100 150 200 250 300 350 400 450 500 550 28.40 28.60 28.80 29.00

30707.D GCMS1126.M Mon Jan 28 11:24:25 2002 Page 10

NYC-WTC_000004452

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NYC-WTC_000004452Source: NYC Law Department, mirrored locally

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