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GCMS analysis results for sample AD30352, Jan 2002

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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30352 conducted on January 10, 2002.

NYC-WTC_000017808–000017832

Folder label: “GCMS X 12/13/01 A 12/27/01

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C : \HPCHEM\ 1 \DATA\DEC2 701\30352.D Vial: 19 Acq On : 28 Dec 2001 5:38 am Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 1-Monolinoleoylglycerol trimet Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T.

28.65 1.67 ug/1 770130 Phenanthrene-dl0 24.98

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1-Monolinoleoylglycerol trimethylsi 498 C27H5404S12 054284-45-6 33 2 Benzoic acid, 2,4-bis (trimethylsil 370 C16H3004Si3 010586-16-0 32 3 Benzeneethanamine, N- (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 25 4 3-Isopropoxy-1,1,1,7,7,7 -hexamethyl 576 C18H5207Si7 071579-69-6 23 Abundance Scan 2572 (28.653 min): 30352.D (-) m/ z 72.9.5 100.00% 73

5000 147 221 281 355 ./Bk Ji / J » y » 11 I । ) 11 i i 11 28.40 28.60 28.80 29.00 1 45 — 117 . 191 249...327,.401429 191 Ma* ■i I 17 it।11 . । » r । i । ....... ............... f . . 1 . । i i > i j i i । < । i * m/z 147.00 35.05% m/z~> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58871:1-Monolinoleoylglycerol trimethylsilyl ether 73 207 5000 147 28.40 28.60 28.80 29.00 34 103 m/z 355.05 20.26% 281 .

m/z-> 50 IPO ' 150 ‘ 200 .95__ 250 300 350 400 450 500 550 Abundance #73975: Benzoic acid, 2.4-bisKtrimethylsilyl)oxy]-. trimet 73 28.40 28.60 28.80 29.00 5000 355 m/z 221.05 19.33% 45 I 133 193 223 281 .. .... ...... m/z-> 50 ioo 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentafluoropheny!)methylene] ' 1 1 1 1 ■ ‘ i ■ ■ 73 355 28.40 28.60 28.80 29.00 m/z 281.00 15.83% 5000

miz-> 45 I 50 208 251.281 386 458 ' ioo ' -150 ‘ 200 ‘ 250 ‘ 300 ' 350 1 ~ 400 ' ‘ 450 ‘ 500 ‘ 550 ' 548 .. n... 28.40 28.60 28.80 29.00

30352.D GCMS1126.M Wed Jan 02 10:50:59 2002 Page 11

NYC-WTC_000017826

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NYC-WTC_000017826Source: NYC Law Department, mirrored locally

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