NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2701\30426.D Vial: 23
Acq On : 28 Dec 2001 11:28 am Operator: 209 GALOS
Sample : GC/MS SCAN 12/13 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 9 1-Monolinoleoylglycerol trimet Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T.
30.25 2.30 ug/1 694473 Chrysene-dl2 33.02
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1-Monolinoleoylglycerol trimethylsi 498 C27H5404S12 054284-45-6 42
2 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 32
3 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 28
4 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 25
Abundance Scan 2746 (30.250 min): 30426.D (-) m/ z 73.00 100.00%
73
5000 147
221 TITI—9——Pm—T/T
281 355 429 30.00 30.20 30.40 30.60
45
■ 1*1 1 ■
96 117.. i
. 1912004—— 249, ..300 327,350. 400
4017450 m/z 147.00 37.68%
miz-> 50 100 150 250
Abundance #58871:1-Monolinoleoylglycerol trimethylsilyl ether
73
207 -----
5000 147 tI
30.00 30.20 30.40 30.60
34 103 m/z 221.05 21.56%
miz-s ' ■ i
50
‘ '
100
i ■ ■ ■ ■
150
i ■ 1 ■ 1
200
1'
1,0201.0009
250 300 350 400
1*T
450
482
Abundance 73
#52459; Trisiloxane. 1,1,1.5,5,5-hexamethyl-3.3-bis[(trimet
147
281 30.00 30.20 30.40 30.60
5000 m/z 355.05 15.16%
207 369
249 £ 338 j
■ ■ i ■ • ■ ■ i ■ ■ ■ 1 t ' ■ ■ 1 i 1 • —I ■ • i ‘ 1 * ■ > • ' 1 ■ i 1 1
m/z-> 50 100 150 200 250 300 350 400 450
Abundance #56714:1.1,1,5>7>7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t
73 30.00 30.20 30.40 30.60
m/z 281.00 13.95%
147
5000 267
355 429
45 207
L| I T I,, J I I | I
i । i i i r [ i . < । > 1 i । > r T-r-n-r ‘ 1 I ‘ '
miz-> 50 100 150 200 250 300 350 400 450 30.00 30.20 30.40 30.60
30426.D GCMS1126.M Wed Jan 02 11:08:15 2002 Page 9
NYC-WTC_000017740
OCR can misread numbers and units. Confirm readings against the page image before using them.