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GCMS analysis results for sample AD30426, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30426 conducted on January 10, 2002.

NYC-WTC_000017724–000017747

Folder label: “GCMS X 12/13/01 A 12/27/01

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Scanned page image, NYC-WTC_000017740
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30426.D Vial: 23 Acq On : 28 Dec 2001 11:28 am Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 1-Monolinoleoylglycerol trimet Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

30.25 2.30 ug/1 694473 Chrysene-dl2 33.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Monolinoleoylglycerol trimethylsi 498 C27H5404S12 054284-45-6 42 2 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 32 3 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 28 4 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 25 Abundance Scan 2746 (30.250 min): 30426.D (-) m/ z 73.00 100.00% 73

5000 147 221 TITI—9——Pm—T/T 281 355 429 30.00 30.20 30.40 30.60 45 ■ 1*1 1 ■ 96 117.. i . 1912004—— 249, ..300 327,350. 400 4017450 m/z 147.00 37.68% miz-> 50 100 150 250 Abundance #58871:1-Monolinoleoylglycerol trimethylsilyl ether 73

207 ----- 5000 147 tI 30.00 30.20 30.40 30.60 34 103 m/z 221.05 21.56%

miz-s ' ■ i 50 ‘ ' 100 i ■ ■ ■ ■ 150 i ■ 1 ■ 1 200 1' 1,0201.0009 250 300 350 400 1*T 450 482

Abundance 73 #52459; Trisiloxane. 1,1,1.5,5,5-hexamethyl-3.3-bis[(trimet 147 281 30.00 30.20 30.40 30.60 5000 m/z 355.05 15.16%

207 369 249 £ 338 j ■ ■ i ■ • ■ ■ i ■ ■ ■ 1 t ' ■ ■ 1 i 1 • —I ■ • i ‘ 1 * ■ > • ' 1 ■ i 1 1 m/z-> 50 100 150 200 250 300 350 400 450 Abundance #56714:1.1,1,5>7>7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t 73 30.00 30.20 30.40 30.60 m/z 281.00 13.95% 147 5000 267 355 429 45 207 L| I T I,, J I I | I i । i i i r [ i . < । > 1 i । > r T-r-n-r ‘ 1 I ‘ ' miz-> 50 100 150 200 250 300 350 400 450 30.00 30.20 30.40 30.60

30426.D GCMS1126.M Wed Jan 02 11:08:15 2002 Page 9

NYC-WTC_000017740

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NYC-WTC_000017740Source: NYC Law Department, mirrored locally

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