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GCMS analysis results for sample AD30351, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.

NYC-WTC_000017833–000017853

Folder label: “GCMS X 12/13/01 A 12/27/01

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30351.D Vial: 20 Acq On : 28 Dec 2001 6:36 am Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 1-Monolinoleoylglycerol trimet Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

30.25 2.20 ug/1 535604 Chrysene-dl2 33.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 42 2 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 36 3 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 32 4 Benzoic acid, 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 30 Abundance Scan 2746 (30.252 min): 30351 .D (-) m/ z 73.00 100.00% 73

5000 147 221 281 355 ‘ ' I Trt i | । i ri । * i i । . 30.00 30.20 30.40 30.60 96 117 . . 191 t . 251., 1 , 327 [ m/z-> ' 45 mr 50 ■ l 1* Pir-'j | 1 •> f |’Ti 1 1 . . 1a . > I r | > 100 150 200 250 300 350 401 Ig 400 450 m/z 147.00 36.23% Abundance #58871:1-Monolinoleoylglycerol trimethylsilyl ether 73

5000 147 207 ■ ' i r C. ■T “ I ■ ' ‘ ‘ I ‘ ‘ 30.00 30.20 30.40 30.60 34 103 m/z 221.05 20.41% । 281 395 - 482 ■ ■ i ■ ■ 1 1 I ■ ■ • ■ i ' ‘ ■ ■ I ' ■ ■ • i ■ 1 • ■ i ■ ■ ■ 1 i ' miz-> 50 100 150 200 250 300 350 400 450 Abundance #56714:1.1.1.5.7.7.7-Heptamethyl-3.3-bis(trimethylsiloxy)t 73 > ' i• • ■ i ' • ■ ■ । ■ 147 30.00 30.20 30.40 30.60 5000 267 m/z 355.05 15.22% 355 429 45 207

I 1***I**1*1* miz-> 50 100 150 200 250 300 350 400 450 Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147 30.00 30.20 30.40 30.60 281 m/z 281.00 13.68% 5000-

369 207 249, 338 L —I ■ 1 i 1 ■ ' ■ i * 1 itb 1 ' i ‘ ‘ ‘ i ‘ 1 ‘ ‘ i ‘ ‘ • i ' 1 m/z—> 50 100 150 200 250 300 350 400 450 30.00 30.20 30.40 30.60

30351.D GCMS1126.M Wed Jan 02 10:46:35 2002 Page 9

NYC-WTC_000017848

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NYC-WTC_000017848Source: NYC Law Department, mirrored locally

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