NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2701\30426.D Vial: 23
Acq On : 28 Dec 2001 11:28 am Operator: 209 GALOS
Sample : GC/MS SCAN 12/13 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 10 1-Monolinoleoylglycerol trimet Concentration Rank 7
R.T. EstConc Area Relative to ISTD R.T.
31.72 2.08 ug/1 628540 Chrys ene-dl2 33.02
Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 45
2 Ethanedioic acid, bis(trimethylsily 234 C8H18O4S12 018294-04-7 32
3 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5S16 038147-00-1 25
4 Butanoic acid, 3-methyl-2-[(trimeth 262 CllH26O3Si2 055124-92-0 23
Abundance Scan 2906 (31.719 min): 30426.D (-) m/z 73.00 100.00%
73
5000 147
221
281 355 31.40 31.60 31.80 32.00 ‘
45 .1 11 1. ', ''191 . 401 429
f ' 249 . 327, I
96 117
m/z-> ' *‘r 1 1 f ri- +r ‘ ' m/z 147.00 41.74%
50 100 150 200 250 300 350 400 450
Abundance #58871:1-Monolinoleoylglycerol trimethylsilyl ether
73
207
5000 147 P—m 1 ' I 1 ' 1 ' I
31.40 31.60 31.80 32.00
34 103
281 m/z 221.0,5 24.05%
| 395
482
IIII
m/z-> 50 100 150 200 250 300 350 400 450
Abundance #71006 Ethanedioic acid, bis trimethyisilyi) ester
73
147
m
31.40 31.60 31.80 32.00
5000 m/z 281.00 17.05%
45
117 190 219
I*I****I**I*
m/z-> 50 100 150 200 250 300 350 400 450
Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsitoxy)t ■ ■ -n • I
73 31.40 31.60 31.80 32.00
m/z 355.05 12.33%
147
5000 267
355 429
45 207
... J, I . ) k
• ’ ■ i ■ • T 1 ‘ ‘ ’ I
miz-> 50 100 ' ' 150 200 250 300 350 400 450
l ‘ ‘ ‘ ' I
31.40 31.60 31.80 32.00
30426.D GCMS1126.M Wed Jan 02 11:08:20 2002 Page 10
NYC-WTC_000017741
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