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GCMS analysis results for sample AD30426, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30426 conducted on January 10, 2002.

NYC-WTC_000017724–000017747

Folder label: “GCMS X 12/13/01 A 12/27/01

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Scanned page image, NYC-WTC_000017741
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30426.D Vial: 23 Acq On : 28 Dec 2001 11:28 am Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 1-Monolinoleoylglycerol trimet Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

31.72 2.08 ug/1 628540 Chrys ene-dl2 33.02

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 45 2 Ethanedioic acid, bis(trimethylsily 234 C8H18O4S12 018294-04-7 32 3 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5S16 038147-00-1 25 4 Butanoic acid, 3-methyl-2-[(trimeth 262 CllH26O3Si2 055124-92-0 23 Abundance Scan 2906 (31.719 min): 30426.D (-) m/z 73.00 100.00% 73

5000 147 221 281 355 31.40 31.60 31.80 32.00 ‘ 45 .1 11 1. ', ''191 . 401 429 f ' 249 . 327, I 96 117 m/z-> ' *‘r 1 1 f ri- +r ‘ ' m/z 147.00 41.74% 50 100 150 200 250 300 350 400 450 Abundance #58871:1-Monolinoleoylglycerol trimethylsilyl ether 73

207 5000 147 P—m 1 ' I 1 ' 1 ' I 31.40 31.60 31.80 32.00 34 103 281 m/z 221.0,5 24.05% | 395 482 IIII m/z-> 50 100 150 200 250 300 350 400 450 Abundance #71006 Ethanedioic acid, bis trimethyisilyi) ester 73

147 m 31.40 31.60 31.80 32.00 5000 m/z 281.00 17.05% 45 117 190 219 I*I****I**I* m/z-> 50 100 150 200 250 300 350 400 450 Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsitoxy)t ■ ■ -n • I 73 31.40 31.60 31.80 32.00 m/z 355.05 12.33% 147 5000 267 355 429 45 207 ... J, I . ) k • ’ ■ i ■ • T 1 ‘ ‘ ’ I miz-> 50 100 ' ' 150 200 250 300 350 400 450 l ‘ ‘ ‘ ' I 31.40 31.60 31.80 32.00

30426.D GCMS1126.M Wed Jan 02 11:08:20 2002 Page 10

NYC-WTC_000017741

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NYC-WTC_000017741Source: NYC Law Department, mirrored locally

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