GCMS analysis results for sample AD30426, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30426.D Vial: 23 Acq On : 28 Dec 2001 11:28 am Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 1-Butanol, 2-ethyl- Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

32.73 0.91 ug/1 274017 Chiysene-dl2 33.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Butanol, 2-ethyl- 102 C6H140 000097-95-0 32 . 2 Propanedioic acid, hexyl-, diethyl 244 C13H2404 005398-10-7 32 3 Butanoic acid, 3-methylbutyl ester 158 C9H18O2 000106-27-4 27 4 trans-3,4-Dimethyl-2-hexene 112 C8H16 019550-82-4 27 Abundance Scan 3016 (32.729 min): 30426.D (-) m/z 57.00 100.00% 57 43 70 112

5000 83 97 —InT —TJOTBT 239 256 32.40 32.60 32.80 33.00 i,I , .129 143 157 171 185 , Il I . i ; p IHouunmufmTTmdTuer 213 - | 16 m/z 112.10 77.47% miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #63557: 1-Butanol, 2-ethyl-

A 43

5000 55 70 ■ ■ i 1 ■ 32.40 32.60 32.80 33.00 31 84 m/z 70.10 76.22% ! -TTTugor 1 ■ i ‘ ' i1 ■ ■11 ■ • ■ ■ i ■ ■ ■ ■ i • ■ ■ ■ i ■ • ■ • i • • ■ ■ i ■1 ■ ■ i • • ■ ■ i ■ ■ m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #32687: Propanedioic acid, hexyl-, diethyl ester 57 70 32.40 32.60 32.80 33.00 5000 112 m/z 43.0 72.07% 83 42 98 1011121’151111-1111-1*11m——m—9u3Ir 199 217 1 i ■ ' ■ ■ i ■ ■ ■ • i ■ ■ ‘ ■ i ‘ 1 miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #67416: Butanoic acid, 3-methylbutyl ester 43 711 32.40 32.60 32.80 33.00 m/z 71.10 69.24% 5000 55 27 89 _1011 miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 32.40 32.60 32.80 33.00

30426.D GCMS1126.M Wed Jan 02 11:08:25 2002 Page 11

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