GCMS sample analysis AD29294, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1001\29295.D Vial: 7 Acq On 12 Dec 2001 5:35 am Operator: 209 GALOS Sample : gc/ms scan 12/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Butanol, 3,3'-oxybis- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

11 ..34 0.81 ug/1 214338 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Butanol, 3,3/-oxybis- 162 C8H18O3 0543.05-61-2 64 2 2-Propanol, (2-methoxy-l-methylet 148 C7H16O3 020324-32-7 56 3 1 -Propanol ,./2 - (2-hydroxypropoxy) - 134 C6H14O3 000106-62-7 45 4 2-Propanol, 1-(2-methoxypropoxy)- 148 C7H1603 013429-07-7 40 Abundance Scan 686 (11.339 min): 29295.D (-) m/z 59.05 100.00% 59

5000-

— 31—51 --- 45 73 103

85............ ।.............................. N 11.00 11.20 11.40 11.60 m/z 44.95 48.14% miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butanol, 3,3‘-oxybis- 59

5000 31 45 103 11.00 11.20 11.40 11.60 m/z 103.05 33.88% ................... 134 1111111111111,11111 —mammm miz—> 20 30 40 50 60 70 80 90 100 110 120 130 140 'Abundance #9238: 2-Propanol, 1 -(2-methoxy-1-methylethoxy- ! 59 i 11.00 11.20 11.40 11.60 5000

miz-> Abundance 20 31

30 I i . TTTE—-TFFr1.1 40 i 45 I

50 60 70 73

........................................ '............... 80 90 #6086: 1-Propanol, 2-(2-hydroxypropoxy)- $ 103 i

100 110 120 130........ 130 140 m/z

11.00 11.20 11-40 11.60 m/z A 73.00 21.131 29.43%

41.05,’' 24.20%

5000

m/z-> 31

40 H 45

> । • ■ । 1 I > > > > । hi ■ । 1 20 30 50 70 7589 —+'I' 1 1 1 i ■ 1 • 1 i ■ • ■ ■ i ■ 60 80 90 103

100 110 120 130 140 J “?1Pr1-fPPITIITT 11.00 11.20 11.40 11.60

29295.D GCMS1126.M Wed Dec 19 12:57:11 2001 Page 2

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