GCMS analysis comments, sample AD28969, Dec 2001

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Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC0701\28969.D Vial: 14 Acq On 8 Dec 2001 3:37 am Operator: 209 GALOS Sample 11/29 gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

11.34 0.94 ug/1 231631 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1/(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 90 2 2-Butanol, 3,3 ' -oxybis- 162 C8H18O3 054305-61-2 64 3 2-Propanol, / 1,1 1 -oxybis- 134 C6H14O3 000110-98-5 56 4 1-Propanol; 2-(2-hydroxypropoxy) - 134 C6H14O3 000106-62-7 53 Abundance Scan 686 (11.344 min): 28969.D (-) m/z 59.05 100.00% 59

5000

• । > ■ ■ > । ■ .31 45

—5051 --- 73 103

130......... N 11.00 11.20 11.40 11.60 m/z 45.00 46.58% mlz-> 20 30 40 60 70 80 90 100 110 120 130 140 Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

5000 103 45 73 11.00 11.20 11.40 11.60 31 m/z 103.05 35.12% ----- —l | ■ ■ • ■ । • .......................... ,........................ 130.......... m/z-> 20 30 40 50 160 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butanol. 3,3‘-oxybis- 59 11.00 11.20 11.40 11.60 5000 m/ z 73.00 29.42%

NA 31 45 103

— ' i ' ' ■ ■ i ■ ................................ 134 m/z-> 20 30 40 50 60 70 80 90 100 11 120 130 140 Abundance #6087: 2-Propanol, 1,1'-oxybis- ■ ' I ■ ' I .-.-, . I 59 11.00 11.20 11.40 11.60 m/ z 41.053, 23.29%

A 31 5000 45 103

m/z-> .. 20 ..401.1. —50IH(60L72. 30 70 80 90 100 110 120 130 140 TTTTTT 11.00 11.20 11.40 11.60

28969.D GCMS1126.M Thu Dec 13 10:28:41 2001 Page 2

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