GCMS analysis comments, sample AD28969, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0701\28969. D Vial: 14 Acq On 8 Dec 2001 3:37 am Operator: 209 GALOS Sample 11/29 gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-1-met Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.43 1.10 ug/1 269973 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1- -methoxy-1-methylet 148 C7H16O3 020324-32-7 83 2 2-Butanol, 3 , ‘-oxybis- 162 C8H18O3 054305-61-2 64 3 2-Propanol, -(2-methoxypropoxy)- 148 C7H1603 013429-07-7 50 4 1-Propanol, 2-(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 45 Abundance Scan 695 (11.427 min): 28969.D (-) m/z 59.05 100.00% 59 5000

39 ■ । > > ■ ■ । ■ 1 ' T TTT 45 73

51 —4 ' ' ' T • ■ । • 85 • • ■ । ■ 103

100 110 120 130 140 i" N 11.00 11.20 11.40 11.60 11.80 m/z 45.00 47.21% m/z-> 20 30 40 50 60 70 80 90 Abundance #9238: 2-Propanol, 1-{2-methoxy-1-methylethoxy)- 59

5000 103 45 11.00 11.20 11.40 11.60 11.80 73 31 m/z 103.00 34.36% ........... ।.......... 130 -------------- —— m/z-> 20 30 40 50 I60 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butanol, 3,3‘-oxybis- 59

11.00 11.20 11.40 11.60 11.80 5000 31 m/z 72.95 26.07% 45 103 । I 1 , I ‘I ' • ■ ' 11 .1 1 1 i 1 1 _ .................. 134 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #9233: 2-Propanol, 1-(2-methoxypropoxy)- 1" 1 [ 1 ’ 1 1 * • ■ I j ■ I » I . I . 59 11.00 11.20 11.40 11.65 11.80 m/z 41.05 22.14%

NUA 5000

31 45

m/Z-> I • l • • • • !'■ ' ‘ I HI 1 20 30 40 - 50 -- 60 70 7—80... 90 194---10— ,. 100 110 120 130 140 11.00 11.20 11.40 11.60 11.80

28969.D GCMS1126.M Thu Dec 13 10:28:46 2001 Page 3

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